tert-butyl (1S,1'S,2S,2'S)-2,2'-thiocarbonylbis(azanediyl)bis(1,2-diphenylethane-2,1-diyl)dicarbamate

Base Information

• Chemical Name: tert-butyl (1S,1'S,2S,2'S)-2,2'-thiocarbonylbis(azanediyl)bis(1,2-diphenylethane-2,1-diyl)dicarbamate
• CAS No.: 1378285-66-5
• Molecular Formula: C₃₉H₄₆N₄O₄S
• Molecular Weight: 666.885

Synonyms:tert-butyl (1S,1'S,2S,2'S)-2,2'-thiocarbonylbis(azanediyl)bis(1,2-diphenylethane-2,1-diyl)dicarbamate

Chemical Property of tert-butyl (1S,1'S,2S,2'S)-2,2'-thiocarbonylbis(azanediyl)bis(1,2-diphenylethane-2,1-diyl)dicarbamate

Chemical Property:

Purity/Quality:

98% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of tert-butyl (1S,1'S,2S,2'S)-2,2'-thiocarbonylbis(azanediyl)bis(1,2-diphenylethane-2,1-diyl)dicarbamate

There total 1 articles about tert-butyl (1S,1'S,2S,2'S)-2,2'-thiocarbonylbis(azanediyl)bis(1,2-diphenylethane-2,1-diyl)dicarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

carbon disulfide (75-15-0,12122-00-8) + tert-Butyl [(1S,2S)-2-amino-1,2-diphenylethyl]carbamate → tert-butyl (1S,1'S,2S,2'S)-2,2'-thiocarbonylbis(azanediyl)bis(1,2-diphenylethane-2,1-diyl)dicarbamate (1378285-66-5)

Guidance literature:

In ethanol; for 20h; Reflux;

DOI:10.1039/c2ob25311a

Reference yield: 80.0%

8-formyl-7-hydroxycoumarin (2067-86-9) + tert-butyl (1S,1'S,2S,2'S)-2,2'-thiocarbonylbis(azanediyl)bis(1,2-diphenylethane-2,1-diyl)dicarbamate (1378285-66-5) → C49H38N4O6S

Guidance literature:

With trifluoroacetic acid; In methanol; dichloromethane; at 20 ℃; for 12h;

DOI:10.1039/c2ob25311a

Reference yield:

tert-butyl (1S,1'S,2S,2'S)-2,2'-thiocarbonylbis(azanediyl)bis(1,2-diphenylethane-2,1-diyl)dicarbamate (1378285-66-5) → C10H17NO4*C49H38N4O6S

Guidance literature:

Multi-step reaction with 2 steps

1: trifluoroacetic acid / methanol; dichloromethane / 12 h / 20 °C

2: toluene

With trifluoroacetic acid; In methanol; dichloromethane; toluene;

DOI:10.1039/c2ob25311a

upstream raw materials:

carbon disulfide

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