1-O-(5-O-acetyl-2,3-di-O-benzoyl-α-D-arabinofuranosyl)trichloroacetimidate

Base Information

Chemical Name:1-O-(5-O-acetyl-2,3-di-O-benzoyl-α-D-arabinofuranosyl)trichloroacetimidate
CAS No.:869216-44-4
Molecular Formula:C₂₃H₂₀Cl₃NO₈
Molecular Weight:544.773
Hs Code.:

Synonyms:1-O-(5-O-acetyl-2,3-di-O-benzoyl-α-D-arabinofuranosyl)trichloroacetimidate

Suppliers and Price of 1-O-(5-O-acetyl-2,3-di-O-benzoyl-α-D-arabinofuranosyl)trichloroacetimidate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of 1-O-(5-O-acetyl-2,3-di-O-benzoyl-α-D-arabinofuranosyl)trichloroacetimidate

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of 1-O-(5-O-acetyl-2,3-di-O-benzoyl-α-D-arabinofuranosyl)trichloroacetimidate

There total 3 articles about 1-O-(5-O-acetyl-2,3-di-O-benzoyl-α-D-arabinofuranosyl)trichloroacetimidate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 5-O-acetyl-2,3-di-O-benzoyl-α-D-arabinofuranose

: 545-06-2
trichloroacetonitrile

: 869216-44-4
1-O-(5-O-acetyl-2,3-di-O-benzoyl-α-D-arabinofuranosyl)trichloroacetimidate

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undec-7-ene; In dichloromethane; at 0 ℃; for 0.166667h;
DOI:10.1093/glycob/cwr068

Reference yield:

: 869216-43-3
C₂₃H₂₂O₉

: 869216-44-4
1-O-(5-O-acetyl-2,3-di-O-benzoyl-α-D-arabinofuranosyl)trichloroacetimidate

Guidance literature:: Multi-step reaction with 2 steps

1: 88 percent / BnNH₂ / tetrahydrofuran / 24 h / 20 °C

2: 86 percent / K₂CO₃ / CH₂Cl₂ / 12 h / 20 °C

With potassium carbonate; benzylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1055/s-2005-872674

Reference yield:

: 869216-42-2
1,2,3-tri-O-benzoyl-5-O-trityl-α-D-arabinofuranose

: 869216-44-4
1-O-(5-O-acetyl-2,3-di-O-benzoyl-α-D-arabinofuranosyl)trichloroacetimidate

Guidance literature:: Multi-step reaction with 3 steps

1: 83 percent / H₂SO₄ / CH₂Cl₂; acetic acid / 12 h / 20 °C

2: 88 percent / BnNH₂ / tetrahydrofuran / 24 h / 20 °C

3: 86 percent / K₂CO₃ / CH₂Cl₂ / 12 h / 20 °C

With sulfuric acid; potassium carbonate; benzylamine; In tetrahydrofuran; dichloromethane; acetic acid;
DOI:10.1055/s-2005-872674