methyl 3-O-benzoyl-1-bromo-1-deoxy-4,5-di-O-mesyl-α-L-sorbopyranoside

Base Information

Chemical Name:methyl 3-O-benzoyl-1-bromo-1-deoxy-4,5-di-O-mesyl-α-L-sorbopyranoside
CAS No.:1025096-36-9
Molecular Formula:C₁₆H₂₁BrO₁₀S₂
Molecular Weight:517.373
Hs Code.:

Synonyms:methyl 3-O-benzoyl-1-bromo-1-deoxy-4,5-di-O-mesyl-α-L-sorbopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl 3-O-benzoyl-1-bromo-1-deoxy-4,5-di-O-mesyl-α-L-sorbopyranoside

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Technology Process of methyl 3-O-benzoyl-1-bromo-1-deoxy-4,5-di-O-mesyl-α-L-sorbopyranoside

There total 4 articles about methyl 3-O-benzoyl-1-bromo-1-deoxy-4,5-di-O-mesyl-α-L-sorbopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 1025096-35-8
methyl 1,3-O-benzylidene-4,5-di-O-mesyl-α-L-sorbopyranoside

: 1025096-36-9
methyl 3-O-benzoyl-1-bromo-1-deoxy-4,5-di-O-mesyl-α-L-sorbopyranoside

Guidance literature:: With N-Bromosuccinimide; barium carbonate; In tetrachloromethane; for 4h; Heating;
DOI:10.1080/10426500701340915

Reference yield:

: 1025096-34-7
methyl 1,3-O-benzylidene-α-L-sorbopyranoside

: 1025096-36-9
methyl 3-O-benzoyl-1-bromo-1-deoxy-4,5-di-O-mesyl-α-L-sorbopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine

2: 80 percent / N-bromosuccinimide; BaCO₃ / CCl₄ / 4 h / Heating

With pyridine; N-Bromosuccinimide; barium carbonate; In tetrachloromethane;
DOI:10.1080/10426500701340915

Reference yield:

: 1125-88-8
benzaldehyde dimethyl acetal

: 1025096-36-9
methyl 3-O-benzoyl-1-bromo-1-deoxy-4,5-di-O-mesyl-α-L-sorbopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 57 percent / camphorsulfonic acid / dimethylformamide / 15 h / 50 °C

2: pyridine

3: 80 percent / N-bromosuccinimide; BaCO₃ / CCl₄ / 4 h / Heating

With pyridine; N-Bromosuccinimide; camphor-10-sulfonic acid; barium carbonate; In tetrachloromethane; N,N-dimethyl-formamide;
DOI:10.1080/10426500701340915