C₂₇H₃₂N₈O₃

Base Information

Chemical Name:C₂₇H₃₂N₈O₃
CAS No.:1612874-00-6
Molecular Formula:C₂₇H₃₂N₈O₃
Molecular Weight:516.603
Hs Code.:

C<sub>27</sub>H<sub>32</sub>N<sub>8</sub>O<sub>3</sub>

Synonyms:C₂₇H₃₂N₈O₃

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Chemical Property of C₂₇H₃₂N₈O₃

Chemical Property:

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Technology Process of C₂₇H₃₂N₈O₃

There total 7 articles about C₂₇H₃₂N₈O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 1612873-97-8
C₁₀H₁₄N₄

: 1612873-99-0
C₁₇H₁₈N₄O₃

: 1612874-00-6
C₂₇H₃₂N₈O₃

Guidance literature:: With sodium 2-(1,2-dihydroxyethyl)-4-hydroxy-5-oxo-2,5-dihydro-furan-3-olate; copper(II) sulfate; In tetrahydrofuran; water; at 20 ℃; for 12h;
DOI:10.1002/ejoc.201301838

Reference yield:

: 1612873-96-7
2-iodo-6-nitro-4-tert-butylaniline

: 1612874-00-6
C₂₇H₃₂N₈O₃

Guidance literature:: Multi-step reaction with 4 steps

1: sodium nitrite; sulfuric acid / ethanol / 0 °C / Reflux

2: tin(II) chloride dihdyrate; ethanol / Reflux

3: sodium azide; sodium 2-(1,2-dihydroxyethyl)-4-hydroxy-5-oxo-2,5-dihydro-furan-3-olate; copper(l) iodide; N,N`-dimethylethylenediamine / dimethyl sulfoxide; water / 1 h / 20 °C

4: sodium 2-(1,2-dihydroxyethyl)-4-hydroxy-5-oxo-2,5-dihydro-furan-3-olate; copper(II) sulfate / water; tetrahydrofuran / 12 h / 20 °C

With copper(l) iodide; sodium azide; sodium 2-(1,2-dihydroxyethyl)-4-hydroxy-5-oxo-2,5-dihydro-furan-3-olate; tin(II) chloride dihdyrate; ethanol; sulfuric acid; copper(II) sulfate; N,N`-dimethylethylenediamine; sodium nitrite; In tetrahydrofuran; ethanol; water; dimethyl sulfoxide;
DOI:10.1002/ejoc.201301838

Reference yield:

: 1369918-94-4
C₁₀H₁₄IN

: 1612874-00-6
C₂₇H₃₂N₈O₃

Guidance literature:: Multi-step reaction with 2 steps

1: sodium azide; sodium 2-(1,2-dihydroxyethyl)-4-hydroxy-5-oxo-2,5-dihydro-furan-3-olate; copper(l) iodide; N,N`-dimethylethylenediamine / dimethyl sulfoxide; water / 1 h / 20 °C

2: sodium 2-(1,2-dihydroxyethyl)-4-hydroxy-5-oxo-2,5-dihydro-furan-3-olate; copper(II) sulfate / water; tetrahydrofuran / 12 h / 20 °C

With copper(l) iodide; sodium azide; sodium 2-(1,2-dihydroxyethyl)-4-hydroxy-5-oxo-2,5-dihydro-furan-3-olate; copper(II) sulfate; N,N`-dimethylethylenediamine; In tetrahydrofuran; water; dimethyl sulfoxide;
DOI:10.1002/ejoc.201301838