5-methyl-1-(trimethylsilyl)hex-1-yn-3-yl (2,4,6-trimethoxyphenyl) carbonate

Base Information

Chemical Name:5-methyl-1-(trimethylsilyl)hex-1-yn-3-yl (2,4,6-trimethoxyphenyl) carbonate
CAS No.:1357013-06-9
Molecular Formula:C₂₀H₃₀O₆Si
Molecular Weight:394.54
Hs Code.:

Synonyms:5-methyl-1-(trimethylsilyl)hex-1-yn-3-yl (2,4,6-trimethoxyphenyl) carbonate

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Chemical Property of 5-methyl-1-(trimethylsilyl)hex-1-yn-3-yl (2,4,6-trimethoxyphenyl) carbonate

Chemical Property:

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Technology Process of 5-methyl-1-(trimethylsilyl)hex-1-yn-3-yl (2,4,6-trimethoxyphenyl) carbonate

There total 3 articles about 5-methyl-1-(trimethylsilyl)hex-1-yn-3-yl (2,4,6-trimethoxyphenyl) carbonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₀H₁₁ClO₅

: 65108-86-3,65108-87-4,80352-60-9
(+/-)-5-methyl-1-(trimethylsilyl)hex-1-yn-3-ol

: 1357013-06-9
5-methyl-1-(trimethylsilyl)hex-1-yn-3-yl (2,4,6-trimethoxyphenyl) carbonate

Guidance literature:: With pyridine; In toluene; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1021/ja300031w

Reference yield:

: 590-86-3
isovaleraldehyde

: 1357013-06-9
5-methyl-1-(trimethylsilyl)hex-1-yn-3-yl (2,4,6-trimethoxyphenyl) carbonate

Guidance literature:: Multi-step reaction with 2 steps

1.1: lithium diisopropyl amide / tetrahydrofuran; n-heptane; ethylbenzene / 0.5 h / 0 - 20 °C / Inert atmosphere

1.2: -78 - 20 °C / Inert atmosphere

1.3: 20 °C / Inert atmosphere

2.1: pyridine / toluene / 0 - 20 °C / Inert atmosphere

With pyridine; lithium diisopropyl amide; In tetrahydrofuran; n-heptane; ethylbenzene; toluene;
DOI:10.1021/ja300031w

Reference yield:

: 1066-54-2
trimethylsilylacetylene

: 1357013-06-9
5-methyl-1-(trimethylsilyl)hex-1-yn-3-yl (2,4,6-trimethoxyphenyl) carbonate

Guidance literature:: Multi-step reaction with 2 steps

1.1: lithium diisopropyl amide / tetrahydrofuran; n-heptane; ethylbenzene / 0.5 h / 0 - 20 °C / Inert atmosphere

1.2: -78 - 20 °C / Inert atmosphere

1.3: 20 °C / Inert atmosphere

2.1: pyridine / toluene / 0 - 20 °C / Inert atmosphere

With pyridine; lithium diisopropyl amide; In tetrahydrofuran; n-heptane; ethylbenzene; toluene;
DOI:10.1021/ja300031w