C₂₆H₃₇O₈N

Base Information

Chemical Name:C₂₆H₃₇O₈N
CAS No.:944455-62-3
Molecular Formula:C₂₆H₃₇NO₈
Molecular Weight:491.582
Hs Code.:

C<sub>26</sub>H<sub>37</sub>O<sub>8</sub>N

Synonyms:C₂₆H₃₇O₈N

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Chemical Property of C₂₆H₃₇O₈N

Chemical Property:

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Technology Process of C₂₆H₃₇O₈N

There total 9 articles about C₂₆H₃₇O₈N which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 944455-61-2
C₂₆H₃₆O₈

: C₂₆H₃₇O₈N

: 944455-62-3
C₂₆H₃₇O₈N

Guidance literature:: With hydroxylamine hydrochloride; In tetrahydrofuran; at 40 ℃; for 24h;
DOI:10.1016/j.tet.2007.02.126

Reference yield:

: 931095-12-4
(2S,3S,4aR,5S,8aR)-2,3-dimethoxy-5-(methoxymethyl)-2,3-dimethyl-2,3,4a,5-tetrahydrobenzo[b][1,4]dioxin-6(8aH)-one

: 944455-62-3
C₂₆H₃₇O₈N

Guidance literature:: Multi-step reaction with 9 steps

1.1: 100 percent / CeCl₃; NaBH₄ / methanol / 0.25 h / 0 °C

2.1: 93 percent / Ph₃P; DEAD / CH₂Cl₂; tetrahydrofuran / 24.5 h / 0 - 4 °C

3.1: 91 percent / TMSCl; triethylamine; LiHMDS / tetrahydrofuran; toluene / 2.5 h / -78 - 20 °C

4.1: toluene; methanol / 20 °C

5.1: 80 percent / DIBAH / CH₂Cl₂ / 3.5 h / -78 °C

6.1: 18-crown-6-ether; KHMDS / tetrahydrofuran / 0.25 h / -78 °C

6.2: 88 percent / tetrahydrofuran / 6 h / -90 - -80 °C

7.1: DIBAH / CH₂Cl₂ / 5 h / -78 °C

8.1: 99 percent / NaHCO₃; Dess-Martin periodinane / CH₂Cl₂ / 20 °C

9.1: 61 percent / hydroxylamine hydrochloride; polymer-supported 2,6-di-tert-butyl-pyridine / tetrahydrofuran / 24 h / 40 °C

With sodium tetrahydroborate; chloro-trimethyl-silane; cerium(III) chloride; 18-crown-6 ether; hydroxylamine hydrochloride; potassium hexamethylsilazane; diisobutylaluminium hydride; sodium hydrogencarbonate; Dess-Martin periodane; triethylamine; triphenylphosphine; lithium hexamethyldisilazane; diethylazodicarboxylate; In tetrahydrofuran; methanol; dichloromethane; toluene; 2.1: Mitsunobu reaction / 6.2: Still-Gennari olefination;
DOI:10.1016/j.tet.2007.02.126

Reference yield:

: 944455-77-0
C₂₅H₃₆O₉

: 944455-62-3
C₂₆H₃₇O₈N

Guidance literature:: Multi-step reaction with 5 steps

1.1: 80 percent / DIBAH / CH₂Cl₂ / 3.5 h / -78 °C

2.1: 18-crown-6-ether; KHMDS / tetrahydrofuran / 0.25 h / -78 °C

2.2: 88 percent / tetrahydrofuran / 6 h / -90 - -80 °C

3.1: DIBAH / CH₂Cl₂ / 5 h / -78 °C

4.1: 99 percent / NaHCO₃; Dess-Martin periodinane / CH₂Cl₂ / 20 °C

5.1: 61 percent / hydroxylamine hydrochloride; polymer-supported 2,6-di-tert-butyl-pyridine / tetrahydrofuran / 24 h / 40 °C

With 18-crown-6 ether; hydroxylamine hydrochloride; potassium hexamethylsilazane; diisobutylaluminium hydride; sodium hydrogencarbonate; Dess-Martin periodane; In tetrahydrofuran; dichloromethane; 2.2: Still-Gennari olefination;
DOI:10.1016/j.tet.2007.02.126