4-(cyclohepta-2,4,6-trien-1-yl)benzoic acid 6-(4-cyclohepta-1,3,6-trien-1-yl-phenoxy)hexyl ester

Base Information

Chemical Name:4-(cyclohepta-2,4,6-trien-1-yl)benzoic acid 6-(4-cyclohepta-1,3,6-trien-1-yl-phenoxy)hexyl ester
CAS No.:216307-01-6
Molecular Formula:C₃₃H₃₄O₃
Molecular Weight:478.631
Hs Code.:

Synonyms:4-(cyclohepta-2,4,6-trien-1-yl)benzoic acid 6-(4-cyclohepta-1,3,6-trien-1-yl-phenoxy)hexyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-(cyclohepta-2,4,6-trien-1-yl)benzoic acid 6-(4-cyclohepta-1,3,6-trien-1-yl-phenoxy)hexyl ester

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of 4-(cyclohepta-2,4,6-trien-1-yl)benzoic acid 6-(4-cyclohepta-1,3,6-trien-1-yl-phenoxy)hexyl ester

There total 4 articles about 4-(cyclohepta-2,4,6-trien-1-yl)benzoic acid 6-(4-cyclohepta-1,3,6-trien-1-yl-phenoxy)hexyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 27.0%

: 216307-00-5
4-(cyclohepta-2,4,6-trien-1-yl)benzoic acid-6-bromo-hexyl ester

: 91902-42-0
7-(4-hydroxyphenyl)-1,3,5-cycloheptatriene

: 216307-01-6
4-(cyclohepta-2,4,6-trien-1-yl)benzoic acid 6-(4-cyclohepta-1,3,6-trien-1-yl-phenoxy)hexyl ester

Guidance literature:: 7-(4-hydroxyphenyl)-1,3,5-cycloheptatriene; With sodium hydride; In N,N-dimethyl-formamide; paraffin oil; at 50 ℃; Inert atmosphere;

4-(cyclohepta-2,4,6-trien-1-yl)benzoic acid-6-bromo-hexyl ester; In N,N-dimethyl-formamide; paraffin oil; at 50 ℃; for 4h; Inert atmosphere;

Reference yield:

: 54615-31-5
1-bromo-4-(cyclohepta-2,4,6-trien-1-yl)benzene

: 216307-01-6
4-(cyclohepta-2,4,6-trien-1-yl)benzoic acid 6-(4-cyclohepta-1,3,6-trien-1-yl-phenoxy)hexyl ester

Guidance literature:: Multi-step reaction with 4 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / -75 °C

1.2: 20 h / -75 - 20 °C

2.1: thionyl chloride / tetrahydrofuran / 4 h / 85 °C

3.1: pyridine / 20 h / 20 °C

4.1: sodium hydride / N,N-dimethyl-formamide; paraffin oil / 50 °C / Inert atmosphere

4.2: 4 h / 50 °C / Inert atmosphere

With pyridine; n-butyllithium; thionyl chloride; sodium hydride; In tetrahydrofuran; hexane; N,N-dimethyl-formamide; paraffin oil;

Reference yield:

: 86318-22-1
4-(cyclohepta-2,4,6-trien-1-yl)benzoic acid

: 216307-01-6
4-(cyclohepta-2,4,6-trien-1-yl)benzoic acid 6-(4-cyclohepta-1,3,6-trien-1-yl-phenoxy)hexyl ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: thionyl chloride / tetrahydrofuran / 4 h / 85 °C

2.1: pyridine / 20 h / 20 °C

3.1: sodium hydride / N,N-dimethyl-formamide; paraffin oil / 50 °C / Inert atmosphere

3.2: 4 h / 50 °C / Inert atmosphere

With pyridine; thionyl chloride; sodium hydride; In tetrahydrofuran; N,N-dimethyl-formamide; paraffin oil;