2,3-Dihydro-7-hydroxy-2-methyl-5-oxo-6-phenyl-5H,3(2H)-pyrrolo<1,2-c>imidazolethione

Base Information

Chemical Name:2,3-Dihydro-7-hydroxy-2-methyl-5-oxo-6-phenyl-5H,3(2H)-pyrrolo<1,2-c>imidazolethione
CAS No.:73384-43-7
Molecular Formula:C₁₃H₁₀N₂O₂S
Molecular Weight:258.301
Hs Code.:

Synonyms:2,3-Dihydro-7-hydroxy-2-methyl-5-oxo-6-phenyl-5H,3(2H)-pyrrolo<1,2-c>imidazolethione

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Chemical Property of 2,3-Dihydro-7-hydroxy-2-methyl-5-oxo-6-phenyl-5H,3(2H)-pyrrolo<1,2-c>imidazolethione

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Technology Process of 2,3-Dihydro-7-hydroxy-2-methyl-5-oxo-6-phenyl-5H,3(2H)-pyrrolo<1,2-c>imidazolethione

There total 3 articles about 2,3-Dihydro-7-hydroxy-2-methyl-5-oxo-6-phenyl-5H,3(2H)-pyrrolo<1,2-c>imidazolethione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 73395-65-0
anhydro-2-Hydroxy-8-methyl-4-oxo-3-phenyl-4H-imidazo<2,1-b><1,3>thiazinium hydroxide

: 73384-43-7
2,3-Dihydro-7-hydroxy-2-methyl-5-oxo-6-phenyl-5H,3(2H)-pyrrolo<1,2-c>imidazolethione

Guidance literature:: In neat (no solvent); at 220 ℃; for 0.0166667h;
DOI:10.1021/jo01300a042

Reference yield:

: 17118-70-6
(chlorocarbonyl)phenyl ketene

: 73384-43-7
2,3-Dihydro-7-hydroxy-2-methyl-5-oxo-6-phenyl-5H,3(2H)-pyrrolo<1,2-c>imidazolethione

Guidance literature:: Multi-step reaction with 3 steps

1: 84 percent / tetrahydrofuran / 12 h / Ambient temperature

2: ethanol; diethyl ether / 24 h / Ambient temperature

3: 100 percent / neat (no solvent) / 0.02 h / 220 °C

In tetrahydrofuran; diethyl ether; ethanol;
DOI:10.1021/jo01300a042

Reference yield:

: 73384-45-9
2-Hydroxy-4-oxo-3-phenyl-4H-imidazo<2,1-b><1,3>thiazine

: 73384-43-7
2,3-Dihydro-7-hydroxy-2-methyl-5-oxo-6-phenyl-5H,3(2H)-pyrrolo<1,2-c>imidazolethione

Guidance literature:: Multi-step reaction with 2 steps

1: ethanol; diethyl ether / 24 h / Ambient temperature

2: 100 percent / neat (no solvent) / 0.02 h / 220 °C

In diethyl ether; ethanol;
DOI:10.1021/jo01300a042