1-cyclododecenylmethyl phenyl sulfide

Base Information

Chemical Name:1-cyclododecenylmethyl phenyl sulfide
CAS No.:125335-03-7
Molecular Formula:C₁₉H₂₈S
Molecular Weight:288.497
Hs Code.:

Synonyms:1-cyclododecenylmethyl phenyl sulfide

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Chemical Property of 1-cyclododecenylmethyl phenyl sulfide

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Technology Process of 1-cyclododecenylmethyl phenyl sulfide

There total 4 articles about 1-cyclododecenylmethyl phenyl sulfide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 69036-34-6
1-(phenylthiomethyl)cyclododecanol

: 125335-03-7
1-cyclododecenylmethyl phenyl sulfide

Guidance literature:: With toluene-4-sulfonic acid; In benzene; Heating;
DOI:10.1016/S0040-4039(00)98638-6

Reference yield:

: 830-13-7
cyclododecanone

: 125335-03-7
1-cyclododecenylmethyl phenyl sulfide

Guidance literature:: Multi-step reaction with 2 steps

1: 89 percent / 1,4-diazabicyclo<2.2.2>octane, n-butyllithium / tetrahydrofuran; hexane / 0 degC for 15 min and room t. for 1.5 h, then 0 degC, 1 h, room t., 1 h

2: 91 percent / p-toluenesulfonic acid / benzene / 7 h / Heating

With 1,4-diaza-bicyclo[2.2.2]octane; n-butyllithium; toluene-4-sulfonic acid; In tetrahydrofuran; hexane; benzene;

Reference yield:

: 13307-75-0
(phenylthio)methyllithium

: 125335-03-7
1-cyclododecenylmethyl phenyl sulfide

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent

2: 100 percent / TsOH / benzene / Heating

With toluene-4-sulfonic acid; In benzene;
DOI:10.1016/S0040-4039(00)98638-6