4,4'-[dithiobis(undecane-11,1-diyloxy)]bis{[N,N-bis(2-pyridylmethyl)aminomethyl]benzene}

Base Information

Chemical Name:4,4'-[dithiobis(undecane-11,1-diyloxy)]bis{[N,N-bis(2-pyridylmethyl)aminomethyl]benzene}
CAS No.:1331961-28-4
Molecular Formula:C₆₀H₈₀N₆O₂S₂
Molecular Weight:981.466
Hs Code.:

Synonyms:4,4'-[dithiobis(undecane-11,1-diyloxy)]bis{[N,N-bis(2-pyridylmethyl)aminomethyl]benzene}

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Chemical Property of 4,4'-[dithiobis(undecane-11,1-diyloxy)]bis{[N,N-bis(2-pyridylmethyl)aminomethyl]benzene}

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Technology Process of 4,4'-[dithiobis(undecane-11,1-diyloxy)]bis{[N,N-bis(2-pyridylmethyl)aminomethyl]benzene}

There total 3 articles about 4,4'-[dithiobis(undecane-11,1-diyloxy)]bis{[N,N-bis(2-pyridylmethyl)aminomethyl]benzene} which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 1539-42-0
bis[(2-pyridyl)methyl]amine

: 180133-73-7
4,4'-[dithiobis(undecane-11,1-diyloxy)]dibenzaldehyde

: 1331961-28-4
4,4'-[dithiobis(undecane-11,1-diyloxy)]bis{[N,N-bis(2-pyridylmethyl)aminomethyl]benzene}

Guidance literature:: With sodium cyanoborohydride; acetic acid; In methanol; at 20 ℃; for 24h; Inert atmosphere;
DOI:10.1007/s11172-011-0044-8

Reference yield:

: 147722-11-0
1,2-bis(11-bromoundecyl)disulfane

: 1331961-28-4
4,4'-[dithiobis(undecane-11,1-diyloxy)]bis{[N,N-bis(2-pyridylmethyl)aminomethyl]benzene}

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / N,N-dimethyl-formamide / 18 h / 60 °C

2: sodium cyanoborohydride; acetic acid / methanol / 24 h / 20 °C / Inert atmosphere

With sodium cyanoborohydride; potassium carbonate; acetic acid; In methanol; N,N-dimethyl-formamide;
DOI:10.1007/s11172-011-0044-8

Reference yield:

: 116129-34-1
11-bromo-1-undecanethiol

: 1331961-28-4
4,4'-[dithiobis(undecane-11,1-diyloxy)]bis{[N,N-bis(2-pyridylmethyl)aminomethyl]benzene}

Guidance literature:: Multi-step reaction with 3 steps

1: iodine / methanol

2: potassium carbonate / N,N-dimethyl-formamide / 18 h / 60 °C

3: sodium cyanoborohydride; acetic acid / methanol / 24 h / 20 °C / Inert atmosphere

With iodine; sodium cyanoborohydride; potassium carbonate; acetic acid; In methanol; N,N-dimethyl-formamide;
DOI:10.1007/s11172-011-0044-8