C₂₅H₂₉IO₆

Base Information

Chemical Name:C₂₅H₂₉IO₆
CAS No.:1362110-54-0
Molecular Formula:C₂₅H₂₉IO₆
Molecular Weight:552.406
Hs Code.:

C<sub>25</sub>H<sub>29</sub>IO<sub>6</sub>

Synonyms:C₂₅H₂₉IO₆

Suppliers and Price of C₂₅H₂₉IO₆

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₂₅H₂₉IO₆

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₂₅H₂₉IO₆

There total 10 articles about C₂₅H₂₉IO₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₅H₃₀O₇

: 1362110-54-0
C₂₅H₂₉IO₆

Guidance literature:: With 1H-imidazole; iodine; triphenylphosphine; In tetrahydrofuran; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1021/ol300390k

Reference yield:

: 1362110-25-5
C₃₂H₄₇IO₄Si

: 1362110-54-0
C₂₅H₂₉IO₆

Guidance literature:: Multi-step reaction with 9 steps

1.1: tert.-butyl lithium / tetrahydrofuran / 0.17 h / -78 °C / Inert atmosphere

1.2: brine

2.1: Burgess Reagent / tetrahydrofuran / 20 - 50 °C / Inert atmosphere

3.1: dichloromethane / 0.33 h / 0 °C / Inert atmosphere

4.1: sodium hydroxide / methanol; water / 0.33 h / 20 °C

5.1: N-chloro-succinimide; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; tetrabutyl-ammonium chloride; sodium hydrogencarbonate; potassium carbonate / dichloromethane / 20 °C / Inert atmosphere

6.1: tetra-(n-butyl)ammonium iodide; sodium hydride / tetrahydrofuran; N,N-dimethyl-formamide / 0.17 h / 0 °C / Inert atmosphere

7.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 20 °C / Inert atmosphere

7.2: brine

8.1: tert.-butylhydroperoxide; bis(acetylacetonate)oxovanadium / dichloromethane / 2 h / 20 °C / Inert atmosphere; Molecular sieve

9.1: 1H-imidazole; iodine; triphenylphosphine / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

With 1H-imidazole; tert.-butylhydroperoxide; N-chloro-succinimide; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; bis(acetylacetonate)oxovanadium; Burgess Reagent; tetrabutyl ammonium fluoride; tetrabutyl-ammonium chloride; iodine; tert.-butyl lithium; tetra-(n-butyl)ammonium iodide; sodium hydride; sodium hydrogencarbonate; potassium carbonate; triphenylphosphine; sodium hydroxide; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide; 1.1: Barbier type cyclization / 8.1: Sharpless epoxidation;
DOI:10.1021/ol300390k

Reference yield:

: C₃₉H₅₁ClO₆Si

: 1362110-54-0
C₂₅H₂₉IO₆

Guidance literature:: Multi-step reaction with 6 steps

1.1: sodium hydroxide / methanol; water / 0.33 h / 20 °C

2.1: N-chloro-succinimide; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; tetrabutyl-ammonium chloride; sodium hydrogencarbonate; potassium carbonate / dichloromethane / 20 °C / Inert atmosphere

3.1: tetra-(n-butyl)ammonium iodide; sodium hydride / tetrahydrofuran; N,N-dimethyl-formamide / 0.17 h / 0 °C / Inert atmosphere

4.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 20 °C / Inert atmosphere

4.2: brine

5.1: tert.-butylhydroperoxide; bis(acetylacetonate)oxovanadium / dichloromethane / 2 h / 20 °C / Inert atmosphere; Molecular sieve

6.1: 1H-imidazole; iodine; triphenylphosphine / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

With 1H-imidazole; tert.-butylhydroperoxide; N-chloro-succinimide; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; bis(acetylacetonate)oxovanadium; tetrabutyl ammonium fluoride; tetrabutyl-ammonium chloride; iodine; tetra-(n-butyl)ammonium iodide; sodium hydride; sodium hydrogencarbonate; potassium carbonate; triphenylphosphine; sodium hydroxide; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide; 5.1: Sharpless epoxidation;
DOI:10.1021/ol300390k