1,13-bis[4'-(4H-chromen-4-on-2-yl)phenyl]-7-(2-chlorobenzyl)-1,4,10,13-tetraoxa-7-azatridecane

Base Information

Chemical Name:1,13-bis[4'-(4H-chromen-4-on-2-yl)phenyl]-7-(2-chlorobenzyl)-1,4,10,13-tetraoxa-7-azatridecane
CAS No.:1346227-46-0
Molecular Formula:C₄₅H₄₀ClNO₈
Molecular Weight:758.267
Hs Code.:

Synonyms:1,13-bis[4'-(4H-chromen-4-on-2-yl)phenyl]-7-(2-chlorobenzyl)-1,4,10,13-tetraoxa-7-azatridecane

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Chemical Property of 1,13-bis[4'-(4H-chromen-4-on-2-yl)phenyl]-7-(2-chlorobenzyl)-1,4,10,13-tetraoxa-7-azatridecane

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Technology Process of 1,13-bis[4'-(4H-chromen-4-on-2-yl)phenyl]-7-(2-chlorobenzyl)-1,4,10,13-tetraoxa-7-azatridecane

There total 4 articles about 1,13-bis[4'-(4H-chromen-4-on-2-yl)phenyl]-7-(2-chlorobenzyl)-1,4,10,13-tetraoxa-7-azatridecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

: 1346226-87-6
1,13-bis[4-(4H-chromen-4-on-2-yl)phenyl]-1,4,10,13-tetraoxa-7-azatridecane

: 611-17-6
1-bromomethyl-2-chlorobenzene

: 1346227-46-0
1,13-bis[4'-(4H-chromen-4-on-2-yl)phenyl]-7-(2-chlorobenzyl)-1,4,10,13-tetraoxa-7-azatridecane

Guidance literature:: With potassium carbonate; In acetonitrile; for 3h; Reflux;

Reference yield:

: 4143-63-9
4'-hydroxyflavone

: 1346227-46-0
1,13-bis[4'-(4H-chromen-4-on-2-yl)phenyl]-7-(2-chlorobenzyl)-1,4,10,13-tetraoxa-7-azatridecane

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 2 h / Reflux

2.1: trifluoroacetic acid / dichloromethane / 2 h / 0 - 20 °C

2.2: pH 10

3.1: potassium carbonate / acetonitrile / 3 h / Reflux

With potassium carbonate; trifluoroacetic acid; In dichloromethane; N,N-dimethyl-formamide; acetonitrile;

Reference yield:

: 1346226-72-9
1,13-bis[4-(4H-chromen-4-on-2-yl)phenyl]-7-(tert-butyloxycarbonyl)-1,4,10,13-tetraoxa-7-azatridecane

: 1346227-46-0
1,13-bis[4'-(4H-chromen-4-on-2-yl)phenyl]-7-(2-chlorobenzyl)-1,4,10,13-tetraoxa-7-azatridecane

Guidance literature:: Multi-step reaction with 2 steps

1.1: trifluoroacetic acid / dichloromethane / 2 h / 0 - 20 °C

1.2: pH 10

2.1: potassium carbonate / acetonitrile / 3 h / Reflux

With potassium carbonate; trifluoroacetic acid; In dichloromethane; acetonitrile;