(R)-N-(1-(4-benzoyl-5-(dimethylamino)thiophen-2-yl)heptyl)-4-methylbenzenesulfonamide

Base Information

Chemical Name:(R)-N-(1-(4-benzoyl-5-(dimethylamino)thiophen-2-yl)heptyl)-4-methylbenzenesulfonamide
CAS No.:1354724-77-8
Molecular Formula:C₂₇H₃₄N₂O₃S₂
Molecular Weight:498.711
Hs Code.:

Synonyms:(R)-N-(1-(4-benzoyl-5-(dimethylamino)thiophen-2-yl)heptyl)-4-methylbenzenesulfonamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (R)-N-(1-(4-benzoyl-5-(dimethylamino)thiophen-2-yl)heptyl)-4-methylbenzenesulfonamide

Chemical Property:

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Technology Process of (R)-N-(1-(4-benzoyl-5-(dimethylamino)thiophen-2-yl)heptyl)-4-methylbenzenesulfonamide

There total 7 articles about (R)-N-(1-(4-benzoyl-5-(dimethylamino)thiophen-2-yl)heptyl)-4-methylbenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₇H₃₆N₂O₄S₂

: 1354724-77-8
(R)-N-(1-(4-benzoyl-5-(dimethylamino)thiophen-2-yl)heptyl)-4-methylbenzenesulfonamide

Guidance literature:: With silica gel; In toluene; at 20 ℃; for 0.166667h;
DOI:10.1021/ol203237r

Reference yield:

: 104504-02-1
4-methyl-N-(tosyloxy)benzenesulfonamide

: 1354724-77-8
(R)-N-(1-(4-benzoyl-5-(dimethylamino)thiophen-2-yl)heptyl)-4-methylbenzenesulfonamide

Guidance literature:: Multi-step reaction with 3 steps

1: (S)-2-{bis[3,5-bis(trifluoromethyl)phenyl][(trimethylsilanyl)oxy]methyl}pyrrolidine; sodium acetate / toluene / 20 h / 20 °C

2: caesium carbonate / toluene / 2 h / 20 °C

3: silica gel / toluene / 0.17 h / 20 °C

With (S)-2-{bis[3,5-bis(trifluoromethyl)phenyl][(trimethylsilanyl)oxy]methyl}pyrrolidine; sodium acetate; silica gel; caesium carbonate; In toluene;
DOI:10.1021/ol203237r

Reference yield:

: 18871-71-1
N,N-dimethyl 3-oxo-3-phenyl-propanamide

: 1354724-77-8
(R)-N-(1-(4-benzoyl-5-(dimethylamino)thiophen-2-yl)heptyl)-4-methylbenzenesulfonamide

Guidance literature:: Multi-step reaction with 3 steps

1: Lawessons reagent / tetrahydrofuran / 20 °C

2: caesium carbonate / toluene / 2 h / 20 °C

3: silica gel / toluene / 0.17 h / 20 °C

With Lawessons reagent; silica gel; caesium carbonate; In tetrahydrofuran; toluene;
DOI:10.1021/ol203237r