methyl (2S)-2-tert-butoxycarbonylamino-5-oxo-8-(diphenylmethyleneimino)nonanoate

Base Information

Chemical Name:methyl (2S)-2-tert-butoxycarbonylamino-5-oxo-8-(diphenylmethyleneimino)nonanoate
CAS No.:871691-86-0
Molecular Formula:C₃₂H₄₂N₂O₇
Molecular Weight:566.695
Hs Code.:

Synonyms:methyl (2S)-2-tert-butoxycarbonylamino-5-oxo-8-(diphenylmethyleneimino)nonanoate

Suppliers and Price of methyl (2S)-2-tert-butoxycarbonylamino-5-oxo-8-(diphenylmethyleneimino)nonanoate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of methyl (2S)-2-tert-butoxycarbonylamino-5-oxo-8-(diphenylmethyleneimino)nonanoate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of methyl (2S)-2-tert-butoxycarbonylamino-5-oxo-8-(diphenylmethyleneimino)nonanoate

There total 2 articles about methyl (2S)-2-tert-butoxycarbonylamino-5-oxo-8-(diphenylmethyleneimino)nonanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 871691-85-9
methyl 5-oxo-2-(tert-butoxycarbonylamino)hept-6-enoate

: 81477-94-3
N-(diphenylmethylene)glycine tert-butyl ester

: 871691-86-0
methyl (2S)-2-tert-butoxycarbonylamino-5-oxo-8-(diphenylmethyleneimino)nonanoate

Guidance literature:: With caesium carbonate; In tetrahydrofuran;
DOI:10.1021/jo0515935

Reference yield:

: 108963-96-8
(S)-1-tert-butoxycarbonyl-5-methoxycarbonyl-pyrrolidin-2-one

: 871691-86-0
methyl (2S)-2-tert-butoxycarbonylamino-5-oxo-8-(diphenylmethyleneimino)nonanoate

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / tetrahydrofuran / 3 h / -40 °C

2: 74 percent / Cs₂CO₃ / tetrahydrofuran

With caesium carbonate; In tetrahydrofuran; 2: Michael addition;
DOI:10.1021/jo0515935

Reference yield:

: 871691-86-0
methyl (2S)-2-tert-butoxycarbonylamino-5-oxo-8-(diphenylmethyleneimino)nonanoate

: (3R,6S,8aR)-6-Amino-5-oxo-octahydro-indolizine-3-carboxylic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 38 percent / AcOH; H₂ / Pd/C / ethanol / 24 h / 1551.44 Torr

2: trifluoroacetic acid; Et₃SiH / CH₂Cl₂ / 1 h

With triethylsilane; hydrogen; acetic acid; trifluoroacetic acid; palladium on activated charcoal; In ethanol; dichloromethane;
DOI:10.1021/jo0515935