isophthalic acid L-alanyl-pyrrolidine L-proline amide

Base Information

Chemical Name:isophthalic acid L-alanyl-pyrrolidine L-proline amide
CAS No.:485835-51-6
Molecular Formula:C₂₀H₂₅N₃O₅
Molecular Weight:387.436
Hs Code.:

Synonyms:isophthalic acid L-alanyl-pyrrolidine L-proline amide

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Chemical Property of isophthalic acid L-alanyl-pyrrolidine L-proline amide

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Technology Process of isophthalic acid L-alanyl-pyrrolidine L-proline amide

There total 3 articles about isophthalic acid L-alanyl-pyrrolidine L-proline amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 485836-64-4
(S)-1-[3-((S)-1-Methyl-2-oxo-2-pyrrolidin-1-yl-ethylcarbamoyl)-benzoyl]-pyrrolidine-2-carboxylic acid methyl ester

: 485835-51-6
isophthalic acid L-alanyl-pyrrolidine L-proline amide

Guidance literature:: With lithium hydroxide; In methanol; at 20 ℃;
DOI:10.1021/jm030811o

Reference yield:

: 485836-63-3
N-(1-methyl-2-oxo-2-pyrrolidin-1-yl-ethyl)-isophthalamic acid methyl ester

: 485835-51-6
isophthalic acid L-alanyl-pyrrolidine L-proline amide

Guidance literature:: Multi-step reaction with 3 steps

1.1: 1.9 g / aq. LiOH / methanol / 20 °C

2.1: pivaloyl chloride; triethylamine / CH₂Cl₂ / 1 h / 0 °C

2.2: triethylamine / CH₂Cl₂ / 20 °C

3.1: 0.76 g / aq. LiOH / methanol / 20 °C

With lithium hydroxide; pivaloyl chloride; triethylamine; In methanol; dichloromethane;
DOI:10.1021/jm030811o

Reference yield:

: 485835-49-2
isophthalic acid mono(L-alanyl-pyrrolidine) amide

: 485835-51-6
isophthalic acid L-alanyl-pyrrolidine L-proline amide

Guidance literature:: Multi-step reaction with 2 steps

1.1: pivaloyl chloride; triethylamine / CH₂Cl₂ / 1 h / 0 °C

1.2: triethylamine / CH₂Cl₂ / 20 °C

2.1: 0.76 g / aq. LiOH / methanol / 20 °C

With lithium hydroxide; pivaloyl chloride; triethylamine; In methanol; dichloromethane;
DOI:10.1021/jm030811o