C₃₅H₄₀O₅Si

Base Information

Chemical Name:C₃₅H₄₀O₅Si
CAS No.:1193357-65-1
Molecular Formula:C₃₅H₄₀O₅Si
Molecular Weight:568.785
Hs Code.:

C<sub>35</sub>H<sub>40</sub>O<sub>5</sub>Si

Synonyms:C₃₅H₄₀O₅Si

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Chemical Property of C₃₅H₄₀O₅Si

Chemical Property:

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Technology Process of C₃₅H₄₀O₅Si

There total 15 articles about C₃₅H₄₀O₅Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 1193357-64-0
C₄₀H₄₈O₇Si

: 1193357-65-1
C₃₅H₄₀O₅Si

Guidance literature:: C₄₀H₄₈O₇Si; With diisobutylaluminium hydride; In hexane; dichloromethane; at -78 ℃; for 1h; Inert atmosphere;

With Rochelle's salt; In hexane; dichloromethane; water; at -78 - 20 ℃; for 1h; Inert atmosphere;
DOI:10.1246/cl.2009.934

Reference yield:

: 1309060-44-3
C₃₁H₄₀O₆S

: 1193357-65-1
C₃₅H₄₀O₅Si

Guidance literature:: Multi-step reaction with 10 steps

1.1: potassium carbonate / methanol / 3 h / 0 °C / Inert atmosphere

2.1: 1H-imidazole / N,N-dimethyl-formamide / 2 h / 0 - 20 °C / Inert atmosphere

3.1: 10 wt% Pd(OH)2 on carbon; hydrogen / ethyl acetate / 6.5 h / 20 °C

4.1: dmap / dichloromethane / 1 h / 20 °C / Inert atmosphere

5.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h / 0 °C / Inert atmosphere

5.2: Inert atmosphere

6.1: tributylphosphine; diamide / toluene / 2.5 h / 0 - 20 °C / Inert atmosphere

7.1: dilithium tetrabromonickelate(II) / tetrahydrofuran; toluene / 18.5 h / 0 °C / Inert atmosphere

8.1: 1H-imidazole / N,N-dimethyl-formamide / 2 h / 0 °C / Inert atmosphere

9.1: N,N,N,N,N,N-hexamethylphosphoric triamide; phenyllithium; phenylmagnesium bromide / tetrahydrofuran; diethyl ether; hexane / 0.5 h / -78 - 0 °C / Inert atmosphere

10.1: diisobutylaluminium hydride / hexane; dichloromethane / 1 h / -78 °C / Inert atmosphere

10.2: 1 h / -78 - 20 °C / Inert atmosphere

With 1H-imidazole; N,N,N,N,N,N-hexamethylphosphoric triamide; dmap; tributylphosphine; dilithium tetrabromonickelate(II); diamide; 10 wt% Pd(OH)2 on carbon; tetrabutyl ammonium fluoride; hydrogen; diisobutylaluminium hydride; potassium carbonate; phenyllithium; phenylmagnesium bromide; In tetrahydrofuran; methanol; diethyl ether; hexane; dichloromethane; ethyl acetate; N,N-dimethyl-formamide; toluene; 6.1: |Mitsunobu Displacement;
DOI:10.1246/cl.2009.934

Reference yield:

: 1193357-62-8
C₃₄H₃₄BrIO₇

: 1193357-65-1
C₃₅H₄₀O₅Si

Guidance literature:: Multi-step reaction with 3 steps

1.1: 1H-imidazole / N,N-dimethyl-formamide / 2 h / 0 °C / Inert atmosphere

2.1: N,N,N,N,N,N-hexamethylphosphoric triamide; phenyllithium; phenylmagnesium bromide / tetrahydrofuran; diethyl ether; hexane / 0.5 h / -78 - 0 °C / Inert atmosphere

3.1: diisobutylaluminium hydride / hexane; dichloromethane / 1 h / -78 °C / Inert atmosphere

3.2: 1 h / -78 - 20 °C / Inert atmosphere

With 1H-imidazole; N,N,N,N,N,N-hexamethylphosphoric triamide; diisobutylaluminium hydride; phenyllithium; phenylmagnesium bromide; In tetrahydrofuran; diethyl ether; hexane; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1246/cl.2009.934