tert-butyl [(1R)-2-amino-1-benzyl-2-(hydroxyimino)-1-methylethyl]carbamate

Base Information

Chemical Name:tert-butyl [(1R)-2-amino-1-benzyl-2-(hydroxyimino)-1-methylethyl]carbamate
CAS No.:868286-29-7
Molecular Formula:C₁₅H₂₃N₃O₃
Molecular Weight:293.366
Hs Code.:

Synonyms:tert-butyl [(1R)-2-amino-1-benzyl-2-(hydroxyimino)-1-methylethyl]carbamate

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Chemical Property of tert-butyl [(1R)-2-amino-1-benzyl-2-(hydroxyimino)-1-methylethyl]carbamate

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Technology Process of tert-butyl [(1R)-2-amino-1-benzyl-2-(hydroxyimino)-1-methylethyl]carbamate

There total 5 articles about tert-butyl [(1R)-2-amino-1-benzyl-2-(hydroxyimino)-1-methylethyl]carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 868286-31-1
C₁₅H₂₀N₂O₂

: 868286-29-7
tert-butyl [(1R)-2-amino-1-benzyl-2-(hydroxyimino)-1-methylethyl]carbamate

Guidance literature:: With hydroxylamine hydrochloride; water; potassium carbonate; isopropyl alcohol; at 130 ℃; for 0.1h; Microwave;

Reference yield:

: 868286-30-0
R-N-(tert-butoxycarbonyl)-α-methylphenylalaninamide

: 868286-29-7
tert-butyl [(1R)-2-amino-1-benzyl-2-(hydroxyimino)-1-methylethyl]carbamate

Guidance literature:: Multi-step reaction with 2 steps

1: Burgess Reagent / 1,2-dichloro-ethane / 0.08 h / 100 °C / Microwave

2: hydroxylamine hydrochloride; water; potassium carbonate; isopropyl alcohol / 0.1 h / 130 °C / Microwave

With Burgess Reagent; hydroxylamine hydrochloride; water; potassium carbonate; isopropyl alcohol; In 1,2-dichloro-ethane;

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 868286-29-7
tert-butyl [(1R)-2-amino-1-benzyl-2-(hydroxyimino)-1-methylethyl]carbamate

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium hydroxide / 1,4-dioxane; water / 14 h

2.1: 1-hydroxy-7-aza-benzotriazole; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 0.5 h / 20 °C

2.2: 0.83 h / -10 °C

3.1: Burgess Reagent / 1,2-dichloro-ethane / 0.08 h / 100 °C / Microwave

4.1: hydroxylamine hydrochloride; water; potassium carbonate; isopropyl alcohol / 0.1 h / 130 °C / Microwave

With sodium hydroxide; 1-hydroxy-7-aza-benzotriazole; Burgess Reagent; hydroxylamine hydrochloride; water; potassium carbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; isopropyl alcohol; In 1,4-dioxane; dichloromethane; water; 1,2-dichloro-ethane;