2-(2-iodophenyl)ethyl methyl 4-methyl-1-phenylpentan-3-yl phosphite

Base Information

• Chemical Name: 2-(2-iodophenyl)ethyl methyl 4-methyl-1-phenylpentan-3-yl phosphite
• CAS No.: 794521-43-0
• Molecular Formula: C₂₁H₂₈IO₃P
• Molecular Weight: 486.33

Synonyms:2-(2-iodophenyl)ethyl methyl 4-methyl-1-phenylpentan-3-yl phosphite

Chemical Property of 2-(2-iodophenyl)ethyl methyl 4-methyl-1-phenylpentan-3-yl phosphite

Chemical Property:

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Technology Process of 2-(2-iodophenyl)ethyl methyl 4-methyl-1-phenylpentan-3-yl phosphite

There total 1 articles about 2-(2-iodophenyl)ethyl methyl 4-methyl-1-phenylpentan-3-yl phosphite which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-(2-iodophenyl)ethan-1-ol (26059-40-5) + phosphorochloridous acid methyl ester 2-methyl-1-phenethyl-propyl ester → 2-(2-iodophenyl)ethyl methyl 4-methyl-1-phenylpentan-3-yl phosphite (794521-43-0)

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; at -78 - 20 ℃;

DOI:10.1021/ja0462777

Reference yield: 90.0%

2-(2-iodophenyl)ethyl methyl 4-methyl-1-phenylpentan-3-yl phosphite (794521-43-0) → isohexylbenzene (4215-86-5) + 1-(2-methyl-1-phenethyl-propoxy)-3,4-dihydro-benzo[c][1,2]oxaphosphinine 1-oxide

Guidance literature:

With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; In benzene; for 2h; Heating;

DOI:10.1021/ja0462777

upstream raw materials:

2-(2-iodophenyl)ethan-1-ol

Downstream raw materials:

isohexylbenzene

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