trideuteriomethyl 2-O-benzoyl-3-O-(2,3,4,6-tetra-O-acetyl-4-O-β-D-galactopyranosyl-3,6-di-O-acetyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)-β-D-galactopyranoside

Base Information

Chemical Name:trideuteriomethyl 2-O-benzoyl-3-O-(2,3,4,6-tetra-O-acetyl-4-O-β-D-galactopyranosyl-3,6-di-O-acetyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)-β-D-galactopyranoside
CAS No.:129579-94-8
Molecular Formula:C₄₆H₅₃NO₂₄
Molecular Weight:1006.9
Hs Code.:

trideuteriomethyl 2-O-benzoyl-3-O-(2,3,4,6-tetra-O-acetyl-4-O-β-D-galactopyranosyl-3,6-di-O-acetyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)-β-D-galactopyranoside

Synonyms:trideuteriomethyl 2-O-benzoyl-3-O-(2,3,4,6-tetra-O-acetyl-4-O-β-D-galactopyranosyl-3,6-di-O-acetyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)-β-D-galactopyranoside

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Chemical Property of trideuteriomethyl 2-O-benzoyl-3-O-(2,3,4,6-tetra-O-acetyl-4-O-β-D-galactopyranosyl-3,6-di-O-acetyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)-β-D-galactopyranoside

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Technology Process of trideuteriomethyl 2-O-benzoyl-3-O-(2,3,4,6-tetra-O-acetyl-4-O-β-D-galactopyranosyl-3,6-di-O-acetyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)-β-D-galactopyranoside

There total 4 articles about trideuteriomethyl 2-O-benzoyl-3-O-(2,3,4,6-tetra-O-acetyl-4-O-β-D-galactopyranosyl-3,6-di-O-acetyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)-β-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 129579-93-7
trideuteriomethyl 2-O-benzoyl-4,6-O-benzylidene-3-O-(2,3,4,6-tetra-O-acetyl-4-O-β-D-galactopyranosyl-3,6-di-O-acetyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)-β-D-galactopyranoside

: 129579-94-8
trideuteriomethyl 2-O-benzoyl-3-O-(2,3,4,6-tetra-O-acetyl-4-O-β-D-galactopyranosyl-3,6-di-O-acetyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)-β-D-galactopyranoside

Guidance literature:: With hydrogen; palladium; In acetic acid; for 16h; Ambient temperature;
DOI:10.1139/v90-147

Reference yield:

: 102717-67-9
C₂₁H₁₉⁽²⁾H₃O₇

: 129579-94-8
trideuteriomethyl 2-O-benzoyl-3-O-(2,3,4,6-tetra-O-acetyl-4-O-β-D-galactopyranosyl-3,6-di-O-acetyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)-β-D-galactopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: silver trifluoromethanesulphonate, 2,6-di-tert-butyl-4-methylpyridine, molecular sieves 3 Angstroem / CH₂Cl₂ / 0-5 deg C to r.t., 16 h

2: 87 percent / H₂ / Pd black / acetic acid / 16 h / Ambient temperature

With 2,6-di-tert-butyl-4-methylpyridine; 3 A molecular sieve; hydrogen; silver trifluoromethanesulfonate; palladium; In dichloromethane; acetic acid;
DOI:10.1139/v90-147

Reference yield:

: 94943-73-4
3,6-di-O-acetyl-4-O-(tetra-O-acetyl-β-D-galactopyranosyl)-2-deoxy-2-phthalimido-α,β-D-glucopyranosyl bromide

: 129579-94-8
trideuteriomethyl 2-O-benzoyl-3-O-(2,3,4,6-tetra-O-acetyl-4-O-β-D-galactopyranosyl-3,6-di-O-acetyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)-β-D-galactopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: silver trifluoromethanesulphonate, 2,6-di-tert-butyl-4-methylpyridine, molecular sieves 3 Angstroem / CH₂Cl₂ / 0-5 deg C to r.t., 16 h

2: 87 percent / H₂ / Pd black / acetic acid / 16 h / Ambient temperature

With 2,6-di-tert-butyl-4-methylpyridine; 3 A molecular sieve; hydrogen; silver trifluoromethanesulfonate; palladium; In dichloromethane; acetic acid;
DOI:10.1139/v90-147