Technology Process of C17H13Cl2N3O2
There total 5 articles about C17H13Cl2N3O2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
tetrabutyl ammonium fluoride;
In
tetrahydrofuran;
at 20 ℃;
for 16h;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: thionyl chloride / chloroform / 18 h / 0 - 20 °C
2: caesium carbonate / N,N-dimethyl-formamide / 18 h / 20 °C
3: tetrabutyl ammonium fluoride / tetrahydrofuran / 16 h / 20 °C
With
thionyl chloride; tetrabutyl ammonium fluoride; caesium carbonate;
In
tetrahydrofuran; chloroform; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 1,4-dioxane / 54 h / 100 °C
2: boron tribromide / dichloromethane / 0.5 h / 0 °C
3: thionyl chloride / chloroform / 18 h / 0 - 20 °C
4: caesium carbonate / N,N-dimethyl-formamide / 18 h / 20 °C
5: tetrabutyl ammonium fluoride / tetrahydrofuran / 16 h / 20 °C
With
thionyl chloride; tetrabutyl ammonium fluoride; boron tribromide; caesium carbonate;
In
tetrahydrofuran; 1,4-dioxane; dichloromethane; chloroform; N,N-dimethyl-formamide;