(Z)-1-(2-(3,4-bis(benzyloxy)-5-oxofuran-2(5H)-ylidene)ethyl)-5-iodopyrimidine-2,4(1H,3H)-dione

Base Information

Chemical Name:(Z)-1-(2-(3,4-bis(benzyloxy)-5-oxofuran-2(5H)-ylidene)ethyl)-5-iodopyrimidine-2,4(1H,3H)-dione
CAS No.:830358-75-3
Molecular Formula:C₂₄H₁₉IN₂O₆
Molecular Weight:558.329
Hs Code.:

Synonyms:(Z)-1-(2-(3,4-bis(benzyloxy)-5-oxofuran-2(5H)-ylidene)ethyl)-5-iodopyrimidine-2,4(1H,3H)-dione

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Chemical Property of (Z)-1-(2-(3,4-bis(benzyloxy)-5-oxofuran-2(5H)-ylidene)ethyl)-5-iodopyrimidine-2,4(1H,3H)-dione

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Technology Process of (Z)-1-(2-(3,4-bis(benzyloxy)-5-oxofuran-2(5H)-ylidene)ethyl)-5-iodopyrimidine-2,4(1H,3H)-dione

There total 2 articles about (Z)-1-(2-(3,4-bis(benzyloxy)-5-oxofuran-2(5H)-ylidene)ethyl)-5-iodopyrimidine-2,4(1H,3H)-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 696-07-1
5-iodouracil

: 231619-90-2
5',6'-di-O-acetyl-2',3'-di-O-benzyl-L-ascorbic acid

: (E)-5-iodouracil-2',3'-di-O-benzyl-4',5'-didehydro-5',6'-dideoxy-L-ascorbic acid

: 830358-75-3
(Z)-1-(2-(3,4-bis(benzyloxy)-5-oxofuran-2(5H)-ylidene)ethyl)-5-iodopyrimidine-2,4(1H,3H)-dione

Guidance literature:: 5',6'-di-O-acetyl-2',3'-di-O-benzyl-L-ascorbic acid; With ammonium sulfate; 1,1,1,3,3,3-hexamethyl-disilazane; Heating;

5-iodouracil; With trimethylsilyl trifluoromethanesulfonate; In acetonitrile; at 60 ℃; Further stages.;
DOI:10.1021/jm070324z

Reference yield:

: 696-07-1
5-iodouracil

: 231619-90-2
5',6'-di-O-acetyl-2',3'-di-O-benzyl-L-ascorbic acid

: 830358-75-3
(Z)-1-(2-(3,4-bis(benzyloxy)-5-oxofuran-2(5H)-ylidene)ethyl)-5-iodopyrimidine-2,4(1H,3H)-dione

Guidance literature:: With ammonium sulfate; trimethylsilyl trifluoromethanesulfonate; 1,1,1,3,3,3-hexamethyl-disilazane; Yield given; Multistep reaction; 1.) reflux, 3 h, 2.) CH₃CN, 12 h;
DOI:10.1021/jm991017z

Reference yield: 72.9%

: 830358-75-3
(Z)-1-(2-(3,4-bis(benzyloxy)-5-oxofuran-2(5H)-ylidene)ethyl)-5-iodopyrimidine-2,4(1H,3H)-dione

: 766-97-2
4-n-methylphenylacetylene

: 1-[5-(p-methylphenylethyn-1''-yl)uracil-1-yl]-2(Z)-(2',3'-di-O-benzyl-2'-buten-4'-olidylidene)ethane

Guidance literature:: With N-ethyl-N,N-diisopropylamine; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In N,N-dimethyl-formamide; at 20 ℃; for 20h;
DOI:10.1021/jm070324z