Technology Process of (E)-((6,10-dimethylundeca-5,9-dien-1-yn-4-yl)sulfonyl)benzene
There total 1 articles about (E)-((6,10-dimethylundeca-5,9-dien-1-yn-4-yl)sulfonyl)benzene which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: N,N-dimethyl-formamide / 6 h / 20 °C / Inert atmosphere
2.1: n-butyllithium / tetrahydrofuran / 0.33 h / -78 °C / Inert atmosphere
2.2: 14 h / -78 - 20 °C / Inert atmosphere
With
n-butyllithium;
In
tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1055/s-0031-1289532
- Guidance literature:
-
With
methanesulfonamide; AD-mix-α;
In
water; tert-butyl alcohol;
at 0 - 20 ℃;
Inert atmosphere;
DOI:10.1055/s-0031-1289532
- Guidance literature:
-
Multi-step reaction with 3 steps
1: AD-mix-α; methanesulfonamide / water; tert-butyl alcohol / 0 - 20 °C / Inert atmosphere
2: SiO2 supported NaIO4 / dichloromethane / 1 h / Inert atmosphere
3: tetrahydrofuran; diethyl ether / 14 h / 0 - 20 °C / Inert atmosphere
With
methanesulfonamide; AD-mix-α;
In
tetrahydrofuran; diethyl ether; dichloromethane; water; tert-butyl alcohol;
DOI:10.1055/s-0031-1289532
