dithiocarbonic acid O-phenethyl ester S-(3,3,3-trifluoro-1-([(4-fluoro-phenyl)-methanesulfonyl-amino]-methyl)-propyl) ester

Base Information

Chemical Name:dithiocarbonic acid O-phenethyl ester S-(3,3,3-trifluoro-1-([(4-fluoro-phenyl)-methanesulfonyl-amino]-methyl)-propyl) ester
CAS No.:339300-32-2
Molecular Formula:C₂₀H₂₁F₄NO₃S₃
Molecular Weight:495.583
Hs Code.:

Synonyms:dithiocarbonic acid O-phenethyl ester S-(3,3,3-trifluoro-1-([(4-fluoro-phenyl)-methanesulfonyl-amino]-methyl)-propyl) ester

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Chemical Property of dithiocarbonic acid O-phenethyl ester S-(3,3,3-trifluoro-1-([(4-fluoro-phenyl)-methanesulfonyl-amino]-methyl)-propyl) ester

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Technology Process of dithiocarbonic acid O-phenethyl ester S-(3,3,3-trifluoro-1-([(4-fluoro-phenyl)-methanesulfonyl-amino]-methyl)-propyl) ester

There total 3 articles about dithiocarbonic acid O-phenethyl ester S-(3,3,3-trifluoro-1-([(4-fluoro-phenyl)-methanesulfonyl-amino]-methyl)-propyl) ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: N-allyl-N-(4-fluorophenyl)methanesulfonamide

: 339300-22-0
dithiocarbonic acid O-phenethyl ester S-trifluoromethyl ester

: 339300-32-2
dithiocarbonic acid O-phenethyl ester S-(3,3,3-trifluoro-1-([(4-fluoro-phenyl)-methanesulfonyl-amino]-methyl)-propyl) ester

Guidance literature:: With dilauryl peroxide; In 1,2-dichloro-ethane; Heating;
DOI:10.1021/ol0156446

Reference yield:

: C₁₁H₉F₃O₂S₂

: 339300-32-2
dithiocarbonic acid O-phenethyl ester S-(3,3,3-trifluoro-1-([(4-fluoro-phenyl)-methanesulfonyl-amino]-methyl)-propyl) ester

Guidance literature:: Multi-step reaction with 2 steps

1: 38 percent / lauroyl peroxide / acetonitrile / Heating

2: 64 percent / lauroyl peroxide / 1,2-dichloro-ethane / Heating

With dilauryl peroxide; In 1,2-dichloro-ethane; acetonitrile;
DOI:10.1021/ol0156446

Reference yield:

: sodium O-phenethyl xanthate

: 339300-32-2
dithiocarbonic acid O-phenethyl ester S-(3,3,3-trifluoro-1-([(4-fluoro-phenyl)-methanesulfonyl-amino]-methyl)-propyl) ester

Guidance literature:: Multi-step reaction with 3 steps

1: acetonitrile / 0.25 h / Heating

2: 38 percent / lauroyl peroxide / acetonitrile / Heating

3: 64 percent / lauroyl peroxide / 1,2-dichloro-ethane / Heating

With dilauryl peroxide; In 1,2-dichloro-ethane; acetonitrile;
DOI:10.1021/ol0156446