2-{3-[3-(2-morpholin-4-yl-ethoxy)phenyl]-[1,2,4]triazolo[4,3-a]pyridin-6-ylsulfanyl}benzylamine

Base Information

• Chemical Name: 2-{3-[3-(2-morpholin-4-yl-ethoxy)phenyl]-[1,2,4]triazolo[4,3-a]pyridin-6-ylsulfanyl}benzylamine
• CAS No.: 946051-03-2
• Molecular Formula: C₂₅H₂₇N₅O₂S
• Molecular Weight: 461.588

Synonyms:2-{3-[3-(2-morpholin-4-yl-ethoxy)phenyl]-[1,2,4]triazolo[4,3-a]pyridin-6-ylsulfanyl}benzylamine

Chemical Property of 2-{3-[3-(2-morpholin-4-yl-ethoxy)phenyl]-[1,2,4]triazolo[4,3-a]pyridin-6-ylsulfanyl}benzylamine

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Technology Process of 2-{3-[3-(2-morpholin-4-yl-ethoxy)phenyl]-[1,2,4]triazolo[4,3-a]pyridin-6-ylsulfanyl}benzylamine

There total 1 articles about 2-{3-[3-(2-morpholin-4-yl-ethoxy)phenyl]-[1,2,4]triazolo[4,3-a]pyridin-6-ylsulfanyl}benzylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

(2-{3-[3-(2-morpholin-4-yl-ethoxy)phenyl]-[1,2,4]triazolo[4,3-a]pyridin-6-ylsulfanyl}benzyl)carbamic acid tert-butyl ester (946051-02-1) → 2-{3-[3-(2-morpholin-4-yl-ethoxy)phenyl]-[1,2,4]triazolo[4,3-a]pyridin-6-ylsulfanyl}benzylamine (946051-03-2)

Guidance literature:

(2-{3-[3-(2-morpholin-4-yl-ethoxy)phenyl]-[1,2,4]triazolo[4,3-a]pyridin-6-ylsulfanyl}benzyl)carbamic acid tert-butyl ester; With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 20h;

With sodium hydroxide; In dichloromethane; water;

Reference yield: 71.0%

phenyl [3-tert-butyl-1-(4-{[tert-butyl(dimethyl)silyl]oxy}-3-chlorophenyl)-1H-pyrazol-5-yl]carbamate (945995-00-6) + 2-{3-[3-(2-morpholin-4-yl-ethoxy)phenyl]-[1,2,4]triazolo[4,3-a]pyridin-6-ylsulfanyl}benzylamine (946051-03-2) → 1-{5-tert-butyl-2-[4-(tert-butyldimethylsilanyloxy)-3-chloro-phenyl]-2H-pyrazol-3-yl}-3-(2-{3-[3-(2-morpholin-4-yl-ethoxy)phenyl]-[1,2,4]triazolo[4,3-a]pyridin-6-ylsulfanyl}benzyl)urea (946051-04-3)

Guidance literature:

In dimethyl sulfoxide; at 20 ℃; for 20h;

upstream raw materials:

(2-{3-[3-(2-morpholin-4-yl-ethoxy)phenyl]-[1,2,4]triazolo[4,3-a]pyridin-6-ylsulfanyl}benzyl)carbamic acid tert-butyl ester

Downstream raw materials:

1-{5-tert-butyl-2-[4-(tert-butyldimethylsilanyloxy)-3-chloro-phenyl]-2H-pyrazol-3-yl}-3-(2-{3-[3-(2-morpholin-4-yl-ethoxy)phenyl]-[1,2,4]triazolo[4,3-a]pyridin-6-ylsulfanyl}benzyl)urea

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