menthyl (1R,4S)-(-)-endo-3-(2-pyridylsulfonyl)bicyclo<2.2.2>oct-5-ene-endo-2-carboxylate

Base Information

Chemical Name:menthyl (1R,4S)-(-)-endo-3-(2-pyridylsulfonyl)bicyclo<2.2.2>oct-5-ene-endo-2-carboxylate
CAS No.:121133-40-2
Molecular Formula:C₂₄H₃₃NO₄S
Molecular Weight:431.596
Hs Code.:

Synonyms:menthyl (1R,4S)-(-)-endo-3-(2-pyridylsulfonyl)bicyclo<2.2.2>oct-5-ene-endo-2-carboxylate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of menthyl (1R,4S)-(-)-endo-3-(2-pyridylsulfonyl)bicyclo<2.2.2>oct-5-ene-endo-2-carboxylate

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Technology Process of menthyl (1R,4S)-(-)-endo-3-(2-pyridylsulfonyl)bicyclo<2.2.2>oct-5-ene-endo-2-carboxylate

There total 2 articles about menthyl (1R,4S)-(-)-endo-3-(2-pyridylsulfonyl)bicyclo<2.2.2>oct-5-ene-endo-2-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 121144-99-8
menthyl (1R,4S)-(+)-(S)_S-endo-3-(2-pyridylsulfinyl)bicyclo<2.2.2>oct-5-ene-endo-2-carboxylate

: 121133-40-2
menthyl (1R,4S)-(-)-endo-3-(2-pyridylsulfonyl)bicyclo<2.2.2>oct-5-ene-endo-2-carboxylate

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; for 5h; Ambient temperature;

Reference yield:

: 105802-70-8,105880-25-9
(Z)-3-<(S)_S-2-pyridylsulphinyl>acrylate

: 121133-40-2
menthyl (1R,4S)-(-)-endo-3-(2-pyridylsulfonyl)bicyclo<2.2.2>oct-5-ene-endo-2-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: 310 mg / anhyd. ZnBr₂ / CH₂Cl₂ / 96 h / Ambient temperature

2: 85 percent / m-chloroperoxybenzoic acid / CH₂Cl₂ / 5 h / Ambient temperature

With 3-chloro-benzenecarboperoxoic acid; zinc dibromide; In dichloromethane;