N-(2-nitrophenyl)sulfonyl-2-(2-(E)-buten-1-yloxy)ethylamine

Base Information

• Chemical Name: N-(2-nitrophenyl)sulfonyl-2-(2-(E)-buten-1-yloxy)ethylamine
• CAS No.: 1361843-53-9
• Molecular Formula: C₁₂H₁₆N₂O₅S
• Molecular Weight: 300.335
• Mol file: 1361843-53-9.mol

Synonyms:N-(2-nitrophenyl)sulfonyl-2-(2-(E)-buten-1-yloxy)ethylamine

Chemical Property of N-(2-nitrophenyl)sulfonyl-2-(2-(E)-buten-1-yloxy)ethylamine

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of N-(2-nitrophenyl)sulfonyl-2-(2-(E)-buten-1-yloxy)ethylamine

There total 1 articles about N-(2-nitrophenyl)sulfonyl-2-(2-(E)-buten-1-yloxy)ethylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

(E)-but-2-enol (504-61-0,542-72-3) + 1-[(2-Nitrophenyl)sulfonyl]aziridine (344951-08-2) → N-(2-nitrophenyl)sulfonyl-2-(2-(E)-buten-1-yloxy)ethylamine (1361843-53-9)

Guidance literature:

(E)-but-2-enol; 1-[(2-Nitrophenyl)sulfonyl]aziridine; In dimethyl sulfoxide; at 20 ℃; for 0.0833333h; Inert atmosphere;

With potassium tert-butylate; In dimethyl sulfoxide; for 4h; Inert atmosphere;

DOI:10.1021/ol300030w

Reference yield: 86.0%

N-(2-nitrophenyl)sulfonyl-2-(2-(E)-buten-1-yloxy)ethylamine (1361843-53-9) → 4-[(2-nitrophenyl)sulfonyl]-3-vinylmorpholine (1361844-09-8)

Guidance literature:

With palladium(II) trifluoroacetate; oxygen; dimethyl sulfoxide; In toluene; at 60 ℃; for 24h; under 3102.97 Torr; Molecular sieve;

DOI:10.1021/ol300030w

upstream raw materials:

(E)-but-2-enol

1-[(2-Nitrophenyl)sulfonyl]aziridine

Downstream raw materials:

4-[(2-nitrophenyl)sulfonyl]-3-vinylmorpholine