<(1β,2β,3β,4β)-4-benzyloxy-3-(tert-butyldiphenylsilyloxymethyl)-2-(fluorocyclopentyl)>amide

Base Information

Chemical Name:<(1β,2β,3β,4β)-4-benzyloxy-3-(tert-butyldiphenylsilyloxymethyl)-2-(fluorocyclopentyl)>amide
CAS No.:135387-47-2
Molecular Formula:C₃₀H₃₆FNO₃Si
Molecular Weight:505.705
Hs Code.:

Synonyms:<(1β,2β,3β,4β)-4-benzyloxy-3-(tert-butyldiphenylsilyloxymethyl)-2-(fluorocyclopentyl)>amide

Suppliers and Price of <(1β,2β,3β,4β)-4-benzyloxy-3-(tert-butyldiphenylsilyloxymethyl)-2-(fluorocyclopentyl)>amide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of <(1β,2β,3β,4β)-4-benzyloxy-3-(tert-butyldiphenylsilyloxymethyl)-2-(fluorocyclopentyl)>amide

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of <(1β,2β,3β,4β)-4-benzyloxy-3-(tert-butyldiphenylsilyloxymethyl)-2-(fluorocyclopentyl)>amide

There total 5 articles about <(1β,2β,3β,4β)-4-benzyloxy-3-(tert-butyldiphenylsilyloxymethyl)-2-(fluorocyclopentyl)>amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 135387-36-9,135500-86-6
<(1β,2β,3β,4β)-4-benzyloxy-2-fluoro-3-(hydroxymethylcyclopentyl)>amide

: 58479-61-1
tert-butylchlorodiphenylsilane

: 135387-47-2
<(1β,2β,3β,4β)-4-benzyloxy-3-(tert-butyldiphenylsilyloxymethyl)-2-(fluorocyclopentyl)>amide

Guidance literature:: With 1H-imidazole; In N,N-dimethyl-formamide; for 4h;

Reference yield: 94.0%

: 135387-36-9,135500-86-6
(1S,2R,3S,4S)-4-Benzyloxy-2-fluoro-3-hydroxymethyl-cyclopentanecarboxylic acid amide

: 58479-61-1
tert-butylchlorodiphenylsilane

: 135387-47-2
(1S,2R,3S,4S)-4-Benzyloxy-3-(tert-butyl-diphenyl-silanyloxymethyl)-2-fluoro-cyclopentanecarboxylic acid amide

Guidance literature:: With 1H-imidazole; In N,N-dimethyl-formamide; for 15h; Ambient temperature;

Reference yield:

: 135387-33-6
5endo-benzyloxy-7anti-fluorobicyclo<2.2.1>heptan-2-one

: 135387-47-2
(1S,2R,3S,4S)-4-Benzyloxy-3-(tert-butyl-diphenyl-silanyloxymethyl)-2-fluoro-cyclopentanecarboxylic acid amide

Guidance literature:: Multi-step reaction with 2 steps

1: 1) meta-chloroperoxybenzoic acid (mCPBA), sodium hydrogencarbonate, 2) liquid ammonia / 1) methylene dichloride, 1-6 h, room temp., 2) 1 h, reflux

2: 94 percent / imidazole / dimethylformamide / 15 h / Ambient temperature

With 1H-imidazole; ammonia; sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid; In N,N-dimethyl-formamide;