2-hydroxy-2-<methyl>acenaphthylen-1-one

Base Information

Chemical Name:2-hydroxy-2-<methyl>acenaphthylen-1-one
CAS No.:138858-23-8
Molecular Formula:C₂₄H₂₃NO₄
Molecular Weight:389.451
Hs Code.:

2-hydroxy-2-<<N-benzyl-N-(carbethoxymethyl)amino>methyl>acenaphthylen-1-one

Synonyms:2-hydroxy-2-<methyl>acenaphthylen-1-one

Suppliers and Price of 2-hydroxy-2-<methyl>acenaphthylen-1-one

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-hydroxy-2-<methyl>acenaphthylen-1-one

Chemical Property:

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Technology Process of 2-hydroxy-2-<methyl>acenaphthylen-1-one

There total 4 articles about 2-hydroxy-2-<methyl>acenaphthylen-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 138858-22-7
N-benzyl-N-<(trimethylsilyl)methyl>glycine ethyl ester

: 6436-90-4
ethyl 2-(benzylamino)acetate

: 138858-29-4
C₂₄H₂₁NO₄

: 138858-23-8
2-hydroxy-2-<methyl>acenaphthylen-1-one

: 138858-24-9
2-hydroxy-2-<amino>carbethoxymethyl>acenaphthylen-1-one

Guidance literature:: With acenaphthene quinone; In acetonitrile; for 2h; Further byproducts given; Irradiation;
DOI:10.1021/jo00031a020

Reference yield:

: 138858-22-7
N-benzyl-N-<(trimethylsilyl)methyl>glycine ethyl ester

: 82-86-0
acenaphthene quinone

: 6436-90-4
ethyl 2-(benzylamino)acetate

: 138858-29-4
C₂₄H₂₁NO₄

: 138858-23-8
2-hydroxy-2-<methyl>acenaphthylen-1-one

: 138858-24-9
2-hydroxy-2-<amino>carbethoxymethyl>acenaphthylen-1-one

Guidance literature:: In methanol; for 2h; Product distribution; Mechanism; Irradiation; other N-benzyl-N-alkylglycine ester, reaction with silyl amines, silylthioether, silylether; influence of oxygen; different solvents and irradiation times;
DOI:10.1021/jo00031a020

Reference yield:

: 103-67-3
benzyl-methyl-amine

: 138858-23-8
2-hydroxy-2-<methyl>acenaphthylen-1-one

Guidance literature:: Multi-step reaction with 2 steps

1: 92.1 percent / acetonitrile / 3 h / 0 °C

2: 21 percent Turnov_. / CH₂Cl₂ / 0.5 h / Irradiation

In dichloromethane; acetonitrile;
DOI:10.1021/jo00031a020