octyl 2-(phenylsulfonyl)acetate

Base Information

• Chemical Name: octyl 2-(phenylsulfonyl)acetate
• CAS No.: 1000817-24-2
• Molecular Formula: C₁₆H₂₄O₄S
• Molecular Weight: 312.43
• Mol file: 1000817-24-2.mol

Synonyms:octyl 2-(phenylsulfonyl)acetate

Chemical Property of octyl 2-(phenylsulfonyl)acetate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of octyl 2-(phenylsulfonyl)acetate

There total 2 articles about octyl 2-(phenylsulfonyl)acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

n-octyl chloroacetate (5451-98-9) + sodium benzenesulfonate (873-55-2) → octyl 2-(phenylsulfonyl)acetate (1000817-24-2)

Guidance literature:

In N,N-dimethyl-formamide; at 20 - 30 ℃; Large scale;

Reference yield:

octanol (111-87-5) → octyl 2-(phenylsulfonyl)acetate (1000817-24-2)

Guidance literature:

Multi-step reaction with 2 steps

1: dichloromethane / 30 - 40 °C / Large scale

2: N,N-dimethyl-formamide / 20 - 30 °C / Large scale

In dichloromethane; N,N-dimethyl-formamide;

Reference yield: 81.0%

octyl 2-(phenylsulfonyl)acetate (1000817-24-2) + N,N,N',N'-tetraethyl-1,5-diazapentadiene tetrafluoroborate → (2E,4E)-5-(diethylamino)-2-(benzenesulfonyl)penta-2,4-dienoic acid octyl ester

Guidance literature:

With 1,8-diazabicyclo[5.4.0]undec-7-ene; In N,N-dimethyl acetamide; at 20 - 30 ℃; Large scale;

upstream raw materials:

octanol

n-octyl chloroacetate

sodium benzenesulfonate

Downstream raw materials:

C₂₇H₃₃NO₅S

Refernces