4-(n-butylamino)-6-(p-fluorophenyl)pyrimido[4,5-b][1,4]benzothiazepine 11-oxide

Base Information

Chemical Name:4-(n-butylamino)-6-(p-fluorophenyl)pyrimido[4,5-b][1,4]benzothiazepine 11-oxide
CAS No.:929034-73-1
Molecular Formula:C₂₁H₁₉FN₄OS
Molecular Weight:394.472
Hs Code.:

Synonyms:4-(n-butylamino)-6-(p-fluorophenyl)pyrimido[4,5-b][1,4]benzothiazepine 11-oxide

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Chemical Property of 4-(n-butylamino)-6-(p-fluorophenyl)pyrimido[4,5-b][1,4]benzothiazepine 11-oxide

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Technology Process of 4-(n-butylamino)-6-(p-fluorophenyl)pyrimido[4,5-b][1,4]benzothiazepine 11-oxide

There total 1 articles about 4-(n-butylamino)-6-(p-fluorophenyl)pyrimido[4,5-b][1,4]benzothiazepine 11-oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 873106-37-7
4-(phenylthio)-6-(p-fluorophenyl)pyrimido[4,5-b][1,4]benzothiazepine

: 929034-73-1
4-(n-butylamino)-6-(p-fluorophenyl)pyrimido[4,5-b][1,4]benzothiazepine 11-oxide

Guidance literature:: Multi-step reaction with 2 steps

1: 52 percent / m-CPBA / CH₂Cl₂ / 8 h / 20 °C

2: 92 percent / CH₂Cl₂ / 0.25 h / 20 °C

With 3-chloro-benzenecarboperoxoic acid; In dichloromethane;
DOI:10.1021/ol0627146