3'-[3,5-bis(trifluoromethyl)phenyl]-1'-(4-nitrophenyl)pyrazolo[4',5'-a][60]fullerene

Base Information

• Chemical Name: 3'-[3,5-bis(trifluoromethyl)phenyl]-1'-(4-nitrophenyl)pyrazolo[4',5'-a][60]fullerene
• CAS No.: 679787-21-4
• Molecular Formula: C₇₅H₇F₆N₃O₂
• Molecular Weight: 1095.89

Synonyms:3'-[3,5-bis(trifluoromethyl)phenyl]-1'-(4-nitrophenyl)pyrazolo[4',5'-a][60]fullerene

Chemical Property of 3'-[3,5-bis(trifluoromethyl)phenyl]-1'-(4-nitrophenyl)pyrazolo[4',5'-a][60]fullerene

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Technology Process of 3'-[3,5-bis(trifluoromethyl)phenyl]-1'-(4-nitrophenyl)pyrazolo[4',5'-a][60]fullerene

There total 2 articles about 3'-[3,5-bis(trifluoromethyl)phenyl]-1'-(4-nitrophenyl)pyrazolo[4',5'-a][60]fullerene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.0%

N-(3,5-bis-trifluoromethyl-benzylidene)-N'-(4-nitrophenyl)hydrazine (767340-09-0) + fullerene-C60 (99685-96-8,161105-99-3,161106-00-9,111138-12-6,133318-63-5,134053-11-5,134931-35-4,134931-36-5,139703-76-7,145633-27-8,175414-73-0,175414-74-1,175414-75-2,175519-12-7,175519-13-8,175519-14-9,175519-15-0,136376-46-0,144906-37-6,144906-38-7,151767-00-9,152882-97-8,152882-98-9,152882-99-0,153062-34-1,154171-74-1,154171-75-2,154333-99-0,154334-00-6,154397-63-4,154460-59-0,199456-56-9,108739-25-9,120329-57-9,120329-58-0) → 3'-[3,5-bis(trifluoromethyl)phenyl]-1'-(4-nitrophenyl)pyrazolo[4',5'-a][60]fullerene (679787-21-4)

Guidance literature:

N-(3,5-bis-trifluoromethyl-benzylidene)-N'-(4-nitrophenyl)hydrazine; With N-Bromosuccinimide; In chloroform; at 20 ℃; for 0.5h;

fullerene-C₆₀; With triethylamine; In toluene; for 0.416667h; microwave irradiation;

DOI:10.1246/bcsj.78.1500

Reference yield:

C15H8BrF6N3O2 (767340-10-3) + fullerene-C60 (99685-96-8,161105-99-3,161106-00-9,111138-12-6,133318-63-5,134053-11-5,134931-35-4,134931-36-5,139703-76-7,145633-27-8,175414-73-0,175414-74-1,175414-75-2,175519-12-7,175519-13-8,175519-14-9,175519-15-0,136376-46-0,144906-37-6,144906-38-7,151767-00-9,152882-97-8,152882-98-9,152882-99-0,153062-34-1,154171-74-1,154171-75-2,154333-99-0,154334-00-6,154397-63-4,154460-59-0,199456-56-9,108739-25-9,120329-57-9,120329-58-0) → 3'-[3,5-bis(trifluoromethyl)phenyl]-1'-(4-nitrophenyl)pyrazolo[4',5'-a][60]fullerene (679787-21-4)

Guidance literature:

With triethylamine; In toluene;

DOI:10.1055/s-2007-977425

Reference yield: 47.0%

3'-[3,5-bis(trifluoromethyl)phenyl]-1'-(4-nitrophenyl)pyrazolo[4',5'-a][60]fullerene (679787-21-4) → C75H6F6N4O4

Guidance literature:

With trifluoromethylsulfonic anhydride; tetramethylammonium nitrate; In dichloromethane; at 20 ℃; for 3h;

DOI:10.1055/s-2007-977425

upstream raw materials:

N-(3,5-bis-trifluoromethyl-benzylidene)-N'-(4-nitrophenyl)hydrazine

fullerene-C₆₀

C₁₅H₈BrF₆N₃O₂

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