Technology Process of C28H32N4O8
There total 5 articles about C28H32N4O8 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
3-chloro-benzenecarboperoxoic acid;
In
dichloromethane;
at 0 - 4 ℃;
for 20h;
DOI:10.1021/ja2104679
- Guidance literature:
-
Multi-step reaction with 4 steps
2.1: potassium carbonate / methanol / 0.17 h / 20 °C
2.2: 2 h / 20 °C
3.1: copper(II) sulfate; sodium L-ascorbate / methanol; water
4.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 20 h / 0 - 4 °C
With
potassium carbonate; copper(II) sulfate; sodium L-ascorbate; 3-chloro-benzenecarboperoxoic acid;
In
methanol; dichloromethane; water;
1.1: Swern oxidation;
DOI:10.1021/ja2104679
- Guidance literature:
-
Multi-step reaction with 2 steps
1: copper(II) sulfate; sodium L-ascorbate / methanol; water
2: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 20 h / 0 - 4 °C
With
copper(II) sulfate; sodium L-ascorbate; 3-chloro-benzenecarboperoxoic acid;
In
methanol; dichloromethane; water;
DOI:10.1021/ja2104679