C₁₈H₁₅N₅O

Base Information

Chemical Name:C₁₈H₁₅N₅O
CAS No.:944149-73-9
Molecular Formula:C₁₈H₁₅N₅O
Molecular Weight:317.35
Hs Code.:

C<sub>18</sub>H<sub>15</sub>N<sub>5</sub>O

Synonyms:C₁₈H₁₅N₅O

Suppliers and Price of C₁₈H₁₅N₅O

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₁₈H₁₅N₅O

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₁₈H₁₅N₅O

There total 7 articles about C₁₈H₁₅N₅O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 944149-25-1
N,N-diallyl-m-phenylenediamine

: 944149-73-9
C₁₈H₁₅N₅O

Guidance literature:: Multi-step reaction with 6 steps

1: 35 percent / toluene / 2 h / 110 °C

2: 95 percent / NEt₃ / dimethylformamide / 4 h

3: 93 percent / NEt₃ / PdCl₂(PPh₃)2; CuI / dimethylformamide / 1 h / 20 °C

4: 66 percent / 1,3-dimethylbarbituric acid / Pd(PPh₃)4 / tetrahydrofuran / 12 h / 65 °C

5: K₂CO₃ / methanol; CH₂Cl₂ / 2 h / 0 - 20 °C

6: tris-benzyltriazolyl amine; sodium ascorbate; CuSO₄ / 2-methyl-propan-2-ol; H₂O; dimethylsulfoxide / 20 h / 70 °C

With 1,3-dimethylbarbituric acid; potassium carbonate; copper(II) sulfate; sodium L-ascorbate; triethylamine; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; methanol; dichloromethane; water; dimethyl sulfoxide; N,N-dimethyl-formamide; toluene; tert-butyl alcohol; 3: Sonogashira reaction;
DOI:10.1021/ja070867y

Reference yield:

: 944149-26-2
C₁₅H₁₆N₂O₂

: 944149-73-9
C₁₈H₁₅N₅O

Guidance literature:: Multi-step reaction with 5 steps

1: 95 percent / NEt₃ / dimethylformamide / 4 h

2: 93 percent / NEt₃ / PdCl₂(PPh₃)2; CuI / dimethylformamide / 1 h / 20 °C

3: 66 percent / 1,3-dimethylbarbituric acid / Pd(PPh₃)4 / tetrahydrofuran / 12 h / 65 °C

4: K₂CO₃ / methanol; CH₂Cl₂ / 2 h / 0 - 20 °C

5: tris-benzyltriazolyl amine; sodium ascorbate; CuSO₄ / 2-methyl-propan-2-ol; H₂O; dimethylsulfoxide / 20 h / 70 °C

With 1,3-dimethylbarbituric acid; potassium carbonate; copper(II) sulfate; sodium L-ascorbate; triethylamine; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; methanol; dichloromethane; water; dimethyl sulfoxide; N,N-dimethyl-formamide; tert-butyl alcohol; 2: Sonogashira reaction;
DOI:10.1021/ja070867y

Reference yield:

: 944149-69-3
C₂₀H₂₄N₂OSi

: 944149-73-9
C₁₈H₁₅N₅O

Guidance literature:: Multi-step reaction with 3 steps

1: 66 percent / 1,3-dimethylbarbituric acid / Pd(PPh₃)4 / tetrahydrofuran / 12 h / 65 °C

2: K₂CO₃ / methanol; CH₂Cl₂ / 2 h / 0 - 20 °C

3: tris-benzyltriazolyl amine; sodium ascorbate; CuSO₄ / 2-methyl-propan-2-ol; H₂O; dimethylsulfoxide / 20 h / 70 °C

With 1,3-dimethylbarbituric acid; potassium carbonate; copper(II) sulfate; sodium L-ascorbate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; methanol; dichloromethane; water; dimethyl sulfoxide; tert-butyl alcohol;
DOI:10.1021/ja070867y