(S)-4-(1-(3-bromo-5-(trifluoromethyl)phenyl)ethyl) 1-tert-butyl 4-phenylpiperidine-1,4-dicarboxylate

Base Information

Chemical Name:(S)-4-(1-(3-bromo-5-(trifluoromethyl)phenyl)ethyl) 1-tert-butyl 4-phenylpiperidine-1,4-dicarboxylate
CAS No.:954124-19-7
Molecular Formula:C₂₆H₂₉BrF₃NO₄
Molecular Weight:556.42
Hs Code.:

Synonyms:(S)-4-(1-(3-bromo-5-(trifluoromethyl)phenyl)ethyl) 1-tert-butyl 4-phenylpiperidine-1,4-dicarboxylate

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Chemical Property of (S)-4-(1-(3-bromo-5-(trifluoromethyl)phenyl)ethyl) 1-tert-butyl 4-phenylpiperidine-1,4-dicarboxylate

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Technology Process of (S)-4-(1-(3-bromo-5-(trifluoromethyl)phenyl)ethyl) 1-tert-butyl 4-phenylpiperidine-1,4-dicarboxylate

There total 1 articles about (S)-4-(1-(3-bromo-5-(trifluoromethyl)phenyl)ethyl) 1-tert-butyl 4-phenylpiperidine-1,4-dicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 954124-13-1
(S)-1-(3-bromo-5-(trifluoromethyl)phenyl)ethanol

: 167262-68-2
N-(t-butyloxycarbonyl)-4-phenylpiperidine-4-carboxylic acid

: 954124-19-7
(S)-4-(1-(3-bromo-5-(trifluoromethyl)phenyl)ethyl) 1-tert-butyl 4-phenylpiperidine-1,4-dicarboxylate

Guidance literature:: N-(t-butyloxycarbonyl)-4-phenylpiperidine-4-carboxylic acid; With dicyclohexyl-carbodiimide; In dichloromethane; toluene; at 0 - 20 ℃; for 0.5h;

(S)-1-(3-bromo-5-(trifluoromethyl)phenyl)ethanol; With dmap; In dichloromethane; toluene; at 0 - 20 ℃; for 72h;

Reference yield: 49.0%

: 954124-19-7
(S)-4-(1-(3-bromo-5-(trifluoromethyl)phenyl)ethyl) 1-tert-butyl 4-phenylpiperidine-1,4-dicarboxylate

: 108-24-7
acetic anhydride

: 954124-22-2
C₂₈H₃₃BrF₃NO₅

Guidance literature:: (S)-4-(1-(3-bromo-5-(trifluoromethyl)phenyl)ethyl) 1-tert-butyl 4-phenylpiperidine-1,4-dicarboxylate; With diisobutylaluminium hydride; In dichloromethane; at -78 ℃; for 1h;

acetic anhydride; With pyridine; dmap; In dichloromethane; at -78 - -10 ℃; for 2h;

With methanol; water; Rochelle's salt; In diethyl ether; dichloromethane;