C₃₅H₅₂O₆Si

Base Information

Chemical Name:C₃₅H₅₂O₆Si
CAS No.:1268455-83-9
Molecular Formula:C₃₅H₅₂O₆Si
Molecular Weight:596.88
Hs Code.:

C<sub>35</sub>H<sub>52</sub>O<sub>6</sub>Si

Synonyms:C₃₅H₅₂O₆Si

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Chemical Property of C₃₅H₅₂O₆Si

Chemical Property:

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Technology Process of C₃₅H₅₂O₆Si

There total 25 articles about C₃₅H₅₂O₆Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1268455-81-7
C₃₅H₅₀O₆Si

: 1268455-83-9
C₃₅H₅₂O₆Si

: C₃₅H₅₂O₆Si

Guidance literature:: With zinc borohydride; In diethyl ether; at -40 ℃; for 24h; optical yield given as %de;
DOI:10.1021/ol1031409

Reference yield:

: 1268455-52-2
C₂₄H₃₈O₄Si

: 1268455-83-9
C₃₅H₅₂O₆Si

: C₃₅H₅₂O₆Si

Guidance literature:: Multi-step reaction with 10 steps

1.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 1.5 h / 20 °C

2.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.5 h / 0 °C

2.2: 0 - 20 °C

3.1: methanol; camphor-10-sulfonic acid / dichloromethane / 12 h / 20 °C

4.1: 1H-imidazole / N,N-dimethyl-formamide / 14.5 h / 50 °C

5.1: methanol; camphor-10-sulfonic acid / dichloromethane / 2 h / 0 °C

6.1: sulfur trioxide pyridine complex; triethylamine / dichloromethane; dimethyl sulfoxide / 0.5 h / 0 °C

7.1: sodium dihydrogenphosphate; sodium chlorite; 2-methyl-but-2-ene / water; tert-butyl alcohol / 1.5 h / 20 °C

8.1: dmap; dicyclohexyl-carbodiimide / dichloromethane / 0 - 20 °C

9.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; hexamethyldistannane; lithium chloride / tetrahydrofuran / 1.5 h / 70 °C

9.2: 3.5 h / 20 °C

10.1: zinc borohydride / diethyl ether / 24 h / -40 °C

With 1H-imidazole; methanol; dmap; sodium chlorite; sodium dihydrogenphosphate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; 2-methyl-but-2-ene; zinc borohydride; camphor-10-sulfonic acid; tetrabutyl ammonium fluoride; hexamethyldistannane; sulfur trioxide pyridine complex; sodium hydride; triethylamine; dicyclohexyl-carbodiimide; lithium chloride; In tetrahydrofuran; diethyl ether; dichloromethane; water; dimethyl sulfoxide; N,N-dimethyl-formamide; mineral oil; tert-butyl alcohol;
DOI:10.1021/ol1031409

Reference yield:

: 1268455-62-4
C₂₁H₃₂O₅Si

: 1268455-83-9
C₃₅H₅₂O₆Si

: C₃₅H₅₂O₆Si

Guidance literature:: Multi-step reaction with 3 steps

1.1: dmap; dicyclohexyl-carbodiimide / dichloromethane / 0 - 20 °C

2.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; hexamethyldistannane; lithium chloride / tetrahydrofuran / 1.5 h / 70 °C

2.2: 3.5 h / 20 °C

3.1: zinc borohydride / diethyl ether / 24 h / -40 °C

With dmap; tetrakis(triphenylphosphine) palladium⁽⁰⁾; zinc borohydride; hexamethyldistannane; dicyclohexyl-carbodiimide; lithium chloride; In tetrahydrofuran; diethyl ether; dichloromethane;
DOI:10.1021/ol1031409