Technology Process of C53H92N6O10Si4
There total 15 articles about C53H92N6O10Si4 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
lithium borohydride;
In
tetrahydrofuran;
at -40 - 20 ℃;
Inert atmosphere;
DOI:10.1021/ja501460j
- Guidance literature:
-
Multi-step reaction with 7 steps
1.1: dichloromethane / 1 h / 20 °C / Inert atmosphere; Molecular sieve
1.2: 2 h / Inert atmosphere; Molecular sieve
2.1: ethanol; water / 8 h / 20 - 90 °C / Inert atmosphere
3.1: pyridine / 1.5 h / 20 °C / Inert atmosphere
4.1: triphenylphosphine; silica gel; water / tetrahydrofuran / 4 h / 20 - 50 °C / Inert atmosphere
5.1: N-ethyl-N,N-diisopropylamine; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate / N,N-dimethyl-formamide / 20 °C / Inert atmosphere
6.1: triethylamine / dichloromethane / 5 h / 20 °C / Inert atmosphere
7.1: lithium borohydride / tetrahydrofuran / -40 - 20 °C / Inert atmosphere
With
pyridine; lithium borohydride; water; silica gel; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; triethylamine; N-ethyl-N,N-diisopropylamine; triphenylphosphine;
In
tetrahydrofuran; ethanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1021/ja501460j
- Guidance literature:
-
Multi-step reaction with 2 steps
1: triethylamine / dichloromethane / 5 h / 20 °C / Inert atmosphere
2: lithium borohydride / tetrahydrofuran / -40 - 20 °C / Inert atmosphere
With
lithium borohydride; triethylamine;
In
tetrahydrofuran; dichloromethane;
DOI:10.1021/ja501460j
