C₂₅H₂₅Cl₂N₅O₄S

Base Information

Chemical Name:C₂₅H₂₅Cl₂N₅O₄S
CAS No.:1416698-81-1
Molecular Formula:C₂₅H₂₅Cl₂N₅O₄S
Molecular Weight:562.477
Hs Code.:

C<sub>25</sub>H<sub>25</sub>Cl<sub>2</sub>N<sub>5</sub>O<sub>4</sub>S

Synonyms:C₂₅H₂₅Cl₂N₅O₄S

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₅H₂₅Cl₂N₅O₄S

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Technology Process of C₂₅H₂₅Cl₂N₅O₄S

There total 13 articles about C₂₅H₂₅Cl₂N₅O₄S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: 1147095-62-2,1147096-65-8
5-chloro-2-(4-(N-(2-chloroacetyl)-S-methylsulfonimidoyl)benzamido)-N-(5-chloropyridin-2-yl)benzamide

: 75-31-0
isopropylamine

: 1416698-81-1
C₂₅H₂₅Cl₂N₅O₄S

Guidance literature:: With potassium iodide; In N,N-dimethyl-formamide; at 25 - 30 ℃; for 12h;
DOI:10.1016/j.ejmech.2012.10.005

Reference yield:

: 114129-35-0
methyl 4-(methylsulfinyl)benzoate

: 1416698-81-1
C₂₅H₂₅Cl₂N₅O₄S

Guidance literature:: Multi-step reaction with 8 steps

1: sodium azide; sulfuric acid / chloroform / 15 h / -20 - 50 °C / Inert atmosphere

2: pyridine / dichloromethane; toluene / 3 h / 15 - 30 °C / Inert atmosphere

3: water; sodium hydroxide / tetrahydrofuran / 3 h / 25 - 30 °C

4: N,N-dimethyl-formamide; oxalyl dichloride / dichloromethane / 3 h / 10 - 30 °C / Inert atmosphere

5: tetrahydrofuran / 2 h / 10 - 30 °C / Inert atmosphere

6: sulfuric acid / 0 - 5 °C

7: triethylamine / tetrahydrofuran / 2 h / 0 - 30 °C

8: potassium iodide / N,N-dimethyl-formamide / 12 h / 25 - 30 °C

With pyridine; sodium azide; oxalyl dichloride; sulfuric acid; water; triethylamine; N,N-dimethyl-formamide; potassium iodide; sodium hydroxide; In tetrahydrofuran; dichloromethane; chloroform; N,N-dimethyl-formamide; toluene;
DOI:10.1016/j.ejmech.2012.10.005

Reference yield:

: 2516-95-2
5-chloro-2-nitrobenzoic acid

: 1416698-81-1
C₂₅H₂₅Cl₂N₅O₄S

Guidance literature:: Multi-step reaction with 6 steps

1: pyridine; trichlorophosphate / acetonitrile / 1 h / 0 - 30 °C / Inert atmosphere

2: tin(II) chloride dihdyrate / ethyl acetate / 2 h / 25 - 30 °C

3: tetrahydrofuran / 2 h / 10 - 30 °C / Inert atmosphere

4: sulfuric acid / 0 - 5 °C

5: triethylamine / tetrahydrofuran / 2 h / 0 - 30 °C

6: potassium iodide / N,N-dimethyl-formamide / 12 h / 25 - 30 °C

With pyridine; tin(II) chloride dihdyrate; sulfuric acid; triethylamine; potassium iodide; trichlorophosphate; In tetrahydrofuran; ethyl acetate; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/j.ejmech.2012.10.005