(2S,3R,4S)-3-(3,4-Dimethoxybenzyloxy)-1-<(1,1-dimethylethyl)diphenylsilyloxy>-2,4-dimethyl-5-phenylthiopentane

Base Information

Chemical Name:(2S,3R,4S)-3-(3,4-Dimethoxybenzyloxy)-1-<(1,1-dimethylethyl)diphenylsilyloxy>-2,4-dimethyl-5-phenylthiopentane
CAS No.:131755-74-3
Molecular Formula:C₃₈H₄₈O₄SSi
Molecular Weight:628.948
Hs Code.:

Synonyms:(2S,3R,4S)-3-(3,4-Dimethoxybenzyloxy)-1-<(1,1-dimethylethyl)diphenylsilyloxy>-2,4-dimethyl-5-phenylthiopentane

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Chemical Property of (2S,3R,4S)-3-(3,4-Dimethoxybenzyloxy)-1-<(1,1-dimethylethyl)diphenylsilyloxy>-2,4-dimethyl-5-phenylthiopentane

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Technology Process of (2S,3R,4S)-3-(3,4-Dimethoxybenzyloxy)-1-<(1,1-dimethylethyl)diphenylsilyloxy>-2,4-dimethyl-5-phenylthiopentane

There total 2 articles about (2S,3R,4S)-3-(3,4-Dimethoxybenzyloxy)-1-<(1,1-dimethylethyl)diphenylsilyloxy>-2,4-dimethyl-5-phenylthiopentane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 131755-73-2
(2S,3R,4S)-3-(3,4-Dimethoxybenzyloxy)-1-<(1,1-dimethylethyl)diphenylsilyloxy>-2,4-dimethyl-5-methylsulfonyloxypentane

: 108-98-5
thiophenol

: 131755-74-3
(2S,3R,4S)-3-(3,4-Dimethoxybenzyloxy)-1-<(1,1-dimethylethyl)diphenylsilyloxy>-2,4-dimethyl-5-phenylthiopentane

Guidance literature:: With sodium hydride; In tetrahydrofuran; N,N-dimethyl-formamide; for 0.75h; Ambient temperature;
DOI:10.1016/S0040-4020(01)85585-X

Reference yield:

: 124582-88-3
(2S,3R,4S)-5-(tert-Butyl-diphenyl-silanyloxy)-3-(3,4-dimethoxy-benzyloxy)-2,4-dimethyl-pentan-1-ol

: 131755-74-3
(2S,3R,4S)-3-(3,4-Dimethoxybenzyloxy)-1-<(1,1-dimethylethyl)diphenylsilyloxy>-2,4-dimethyl-5-phenylthiopentane

Guidance literature:: Multi-step reaction with 2 steps

1: 96 percent / CH₂Cl₂ / 14 h / Ambient temperature

2: 89 percent / NaH / tetrahydrofuran; dimethylformamide / 0.75 h / Ambient temperature

With sodium hydride; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4020(01)85585-X