(S)-1-(p-chlorophenylsulfinyl)-2-heptadecanone

Base Information

Chemical Name:(S)-1-(p-chlorophenylsulfinyl)-2-heptadecanone
CAS No.:118133-51-0
Molecular Formula:C₂₃H₃₇ClO₂S
Molecular Weight:413.065
Hs Code.:

Synonyms:(S)-1-(p-chlorophenylsulfinyl)-2-heptadecanone

Suppliers and Price of (S)-1-(p-chlorophenylsulfinyl)-2-heptadecanone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-1-(p-chlorophenylsulfinyl)-2-heptadecanone

Chemical Property:

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Technology Process of (S)-1-(p-chlorophenylsulfinyl)-2-heptadecanone

There total 2 articles about (S)-1-(p-chlorophenylsulfinyl)-2-heptadecanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 19218-94-1
1-iodotetradecane

: 118204-67-4
(S)-1-((4-chlorophenyl)sulfinyl)propan-2-one

: 118133-51-0
(S)-1-(p-chlorophenylsulfinyl)-2-heptadecanone

Guidance literature:: With n-butyllithium; sodium hydride; In tetrahydrofuran; hexane; at 0 ℃; for 3h;
DOI:10.1246/bcsj.61.1273

Reference yield:

: 17530-95-9
1-(4-chlorophenylsulfinyl)propan-2-one

: 118133-51-0
(S)-1-(p-chlorophenylsulfinyl)-2-heptadecanone

Guidance literature:: Multi-step reaction with 2 steps

1: 38 percent / bakers' yeast / aq. ethanol / 12 h

2: 61 percent / sodium hydride, butyllithium / tetrahydrofuran; hexane / 3 h / 0 °C

With n-butyllithium; bakers' yeast; sodium hydride; In tetrahydrofuran; ethanol; hexane;
DOI:10.1246/bcsj.61.1273

Reference yield:

: 118133-51-0
(S)-1-(p-chlorophenylsulfinyl)-2-heptadecanone

: 118133-56-5
(2R)-1-<(S)-p-chlorophenylsulfinyl>-2-heptadecanol

: 118133-61-2
(2S)-1-<(S)-p-chlorophenylsulfinyl>-2-heptadecanol

Guidance literature:: With Diisobutylammonium hydride; In tetrahydrofuran; hexane; at -90 ℃; for 5h; Yield given. Yields of byproduct given;
DOI:10.1246/bcsj.61.1273