p.toluenesulfonyloxy-4β methoxymethylenoxy-6 N,N-dimethylcarboxamidomethyl-9bβ hexahydrodibenzofuranne

Base Information

Chemical Name:p.toluenesulfonyloxy-4β methoxymethylenoxy-6 N,N-dimethylcarboxamidomethyl-9bβ hexahydrodibenzofuranne
CAS No.:117570-29-3
Molecular Formula:C₂₅H₃₁NO₇S
Molecular Weight:489.59
Hs Code.:

Synonyms:p.toluenesulfonyloxy-4β methoxymethylenoxy-6 N,N-dimethylcarboxamidomethyl-9bβ hexahydrodibenzofuranne

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Chemical Property of p.toluenesulfonyloxy-4β methoxymethylenoxy-6 N,N-dimethylcarboxamidomethyl-9bβ hexahydrodibenzofuranne

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Technology Process of p.toluenesulfonyloxy-4β methoxymethylenoxy-6 N,N-dimethylcarboxamidomethyl-9bβ hexahydrodibenzofuranne

There total 4 articles about p.toluenesulfonyloxy-4β methoxymethylenoxy-6 N,N-dimethylcarboxamidomethyl-9bβ hexahydrodibenzofuranne which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 108275-35-0,117569-96-7,117570-18-0
hydroxy-4β methoxymethylenoxy-6 N,N-dimethylcarboxamidomethyl-9bβ hexahydrodibenzofuranne

: 98-59-9
p-toluenesulfonyl chloride

: 117570-29-3
p.toluenesulfonyloxy-4β methoxymethylenoxy-6 N,N-dimethylcarboxamidomethyl-9bβ hexahydrodibenzofuranne

Guidance literature:: In tetrahydrofuran; pyridine; at 40 ℃; for 48h;
DOI:10.1016/S0040-4020(01)85897-X

Reference yield:

: oxo-4 methoxymethylenoxy-6 N,N-dimethylcarboxamidomethyl-9bβ hexahydrodibenzofuranne

: 117570-29-3
p.toluenesulfonyloxy-4β methoxymethylenoxy-6 N,N-dimethylcarboxamidomethyl-9bβ hexahydrodibenzofuranne

Guidance literature:: Multi-step reaction with 2 steps

1: NaBH₄ / methanol

2: 90 percent / pyridine; tetrahydrofuran / 48 h / 40 °C

With sodium tetrahydroborate; In tetrahydrofuran; pyridine; methanol;
DOI:10.1016/S0040-4020(01)85897-X

Reference yield:

: 117569-99-0
(bis-methoxymethylenoxy-2',3' phenyl)-1 (cyclohexene-2 yl)-1 N,N-dimethylacetamide

: 117570-29-3
p.toluenesulfonyloxy-4β methoxymethylenoxy-6 N,N-dimethylcarboxamidomethyl-9bβ hexahydrodibenzofuranne

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) trichloroacetonitrile, KHCO₃, 30 percent H₂O₂ / CH₂Cl₂ / Heating; 1.) r.t., 10 h; 2.) reflux, 10 h

2: 90 percent / pyridine; tetrahydrofuran / 48 h / 40 °C

With dihydrogen peroxide; potassium hydrogencarbonate; trichloroacetonitrile; In tetrahydrofuran; pyridine; dichloromethane;
DOI:10.1016/S0040-4020(01)85897-X