Technology Process of C18H26N2S
There total 5 articles about C18H26N2S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C26H34N2OS;
With
trifluoroacetic acid;
for 5h;
Heating / reflux;
With
sodium hydrogencarbonate;
In
water; ethyl acetate;
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: potassium hydroxide / ethanol / 2 h / Reflux
2.1: pyridine / 2 h / Reflux
3.1: iron; acetic acid / water / 4 h / Reflux
4.1: acetic acid / dichloromethane / 0.08 h / Inert atmosphere
4.2: 1 h / 20 °C
5.1: acetic acid / 6 h / Reflux
6.1: trifluoroacetic acid / 5 h / Reflux
With
pyridine; iron; acetic acid; trifluoroacetic acid; potassium hydroxide;
In
ethanol; dichloromethane; water;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: pyridine / 2 h / Reflux
2.1: iron; acetic acid / water / 4 h / Reflux
3.1: acetic acid / dichloromethane / 0.08 h / Inert atmosphere
3.2: 1 h / 20 °C
4.1: acetic acid / 6 h / Reflux
5.1: trifluoroacetic acid / 5 h / Reflux
With
pyridine; iron; acetic acid; trifluoroacetic acid;
In
dichloromethane; water;