(3S,5S)-1-benzyl-3-allyl-4-tert-butoxycarbonyl-5-methyl-2-oxopiperazine

Base Information

Chemical Name:(3S,5S)-1-benzyl-3-allyl-4-tert-butoxycarbonyl-5-methyl-2-oxopiperazine
CAS No.:1004286-94-5
Molecular Formula:C₂₀H₂₈N₂O₃
Molecular Weight:344.454
Hs Code.:

Synonyms:(3S,5S)-1-benzyl-3-allyl-4-tert-butoxycarbonyl-5-methyl-2-oxopiperazine

Suppliers and Price of (3S,5S)-1-benzyl-3-allyl-4-tert-butoxycarbonyl-5-methyl-2-oxopiperazine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (3S,5S)-1-benzyl-3-allyl-4-tert-butoxycarbonyl-5-methyl-2-oxopiperazine

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Technology Process of (3S,5S)-1-benzyl-3-allyl-4-tert-butoxycarbonyl-5-methyl-2-oxopiperazine

There total 1 articles about (3S,5S)-1-benzyl-3-allyl-4-tert-butoxycarbonyl-5-methyl-2-oxopiperazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 1004286-93-4
tert-butyl (S)-4-benzyl-2-methyl-5-oxopiperazine-1-carboxylate

: 106-95-6
allyl bromide

: 1004286-94-5
(3S,5S)-1-benzyl-3-allyl-4-tert-butoxycarbonyl-5-methyl-2-oxopiperazine

Guidance literature:: tert-butyl (S)-4-benzyl-2-methyl-5-oxopiperazine-1-carboxylate; With N,N,N,N,N,N-hexamethylphosphoric triamide; tert.-butyl lithium; In tetrahydrofuran; pentane; at -78 ℃; for 0.25h;

allyl bromide; In tetrahydrofuran; pentane; at -78 ℃; for 3h; Further stages.;
DOI:10.1016/j.tetasy.2007.10.027

Reference yield: 33.0%

: 1004286-94-5
(3S,5S)-1-benzyl-3-allyl-4-tert-butoxycarbonyl-5-methyl-2-oxopiperazine

: 106-95-6
allyl bromide

: 1004287-00-6
(S)-1-benzyl-3,3-diallyl-4-tert-butoxycarbonyl-5-methyl-2-oxopiperazine

Guidance literature:: (3S,5S)-1-benzyl-3-allyl-4-tert-butoxycarbonyl-5-methyl-2-oxopiperazine; With N,N,N,N,N,N-hexamethylphosphoric triamide; tert.-butyl lithium; In tetrahydrofuran; pentane; at -78 ℃; for 0.25h;

allyl bromide; In tetrahydrofuran; pentane; at -78 ℃; for 2h; Further stages.;
DOI:10.1016/j.tetasy.2007.10.027