(E)-2-({4-bromo-2-[(E)-(hydroxyimino)methyl]phenoxy}methyl)-3-phenylacrylonitrile

Base Information

Chemical Name:(E)-2-({4-bromo-2-[(E)-(hydroxyimino)methyl]phenoxy}methyl)-3-phenylacrylonitrile
CAS No.:1373931-22-6
Molecular Formula:C₁₇H₁₃BrN₂O₂
Molecular Weight:357.206
Hs Code.:

Synonyms:(E)-2-({4-bromo-2-[(E)-(hydroxyimino)methyl]phenoxy}methyl)-3-phenylacrylonitrile

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Chemical Property of (E)-2-({4-bromo-2-[(E)-(hydroxyimino)methyl]phenoxy}methyl)-3-phenylacrylonitrile

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Technology Process of (E)-2-({4-bromo-2-[(E)-(hydroxyimino)methyl]phenoxy}methyl)-3-phenylacrylonitrile

There total 3 articles about (E)-2-({4-bromo-2-[(E)-(hydroxyimino)methyl]phenoxy}methyl)-3-phenylacrylonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: C₁₇H₁₂BrNO₂

: 1373931-22-6
(E)-2-({4-bromo-2-[(E)-(hydroxyimino)methyl]phenoxy}methyl)-3-phenylacrylonitrile

Guidance literature:: With hydroxylamine hydrochloride; sodium hydroxide; In ethanol; water; at 20 ℃; for 1.5h;
DOI:10.1055/s-0031-1289707

Reference yield:

: 139413-81-3
(E)-2-(bromomethyl)-3-phenylacrylonitrile

: 1373931-22-6
(E)-2-({4-bromo-2-[(E)-(hydroxyimino)methyl]phenoxy}methyl)-3-phenylacrylonitrile

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / acetonitrile / 3 h / 20 °C

2: hydroxylamine hydrochloride; sodium hydroxide / ethanol; water / 1.5 h / 20 °C

With hydroxylamine hydrochloride; potassium carbonate; sodium hydroxide; In ethanol; water; acetonitrile;
DOI:10.1055/s-0031-1289707

Reference yield:

: 1761-61-1
5-bromosalicyclaldehyde

: 1373931-22-6
(E)-2-({4-bromo-2-[(E)-(hydroxyimino)methyl]phenoxy}methyl)-3-phenylacrylonitrile

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / acetonitrile / 3 h / 20 °C

2: hydroxylamine hydrochloride; sodium hydroxide / ethanol; water / 1.5 h / 20 °C

With hydroxylamine hydrochloride; potassium carbonate; sodium hydroxide; In ethanol; water; acetonitrile;
DOI:10.1055/s-0031-1289707