Technology Process of C26H16B2N2O8
There total 4 articles about C26H16B2N2O8 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C38H36B2N2O8;
With
sodium periodate;
In
tetrahydrofuran; water;
at 20 ℃;
for 2h;
With
hydrogenchloride;
In
tetrahydrofuran; water;
at 20 ℃;
for 18h;
DOI:10.1002/anie.201107070
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: 1,3-bis[(diphenylphosphino)propane]dichloronickel(II); N-ethyl-N,N-diisopropylamine / toluene / 12 h / 100 °C / Inert atmosphere
2.1: sodium periodate / tetrahydrofuran; water / 2 h / 20 °C
2.2: 18 h / 20 °C
With
sodium periodate; 1,3-bis[(diphenylphosphino)propane]dichloronickel(II); N-ethyl-N,N-diisopropylamine;
In
tetrahydrofuran; water; toluene;
DOI:10.1002/anie.201107070
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: propionic acid / 18 h / 140 °C / Inert atmosphere
2.1: 1,3-bis[(diphenylphosphino)propane]dichloronickel(II); N-ethyl-N,N-diisopropylamine / toluene / 12 h / 100 °C / Inert atmosphere
3.1: sodium periodate / tetrahydrofuran; water / 2 h / 20 °C
3.2: 18 h / 20 °C
With
sodium periodate; 1,3-bis[(diphenylphosphino)propane]dichloronickel(II); propionic acid; N-ethyl-N,N-diisopropylamine;
In
tetrahydrofuran; water; toluene;
DOI:10.1002/anie.201107070