methyl (4-acetylamino-5-{[(2S)-3-(5-chloro-1'H,3H-spiro[1-benzofuran-2,4'-piperidin]-1'-yl)-2-hydroxypropyl]oxy}phenoxy)acetate

Base Information

Chemical Name:methyl (4-acetylamino-5-{[(2S)-3-(5-chloro-1'H,3H-spiro[1-benzofuran-2,4'-piperidin]-1'-yl)-2-hydroxypropyl]oxy}phenoxy)acetate
CAS No.:1003567-22-3
Molecular Formula:C₂₆H₃₁ClN₂O₇
Molecular Weight:518.994
Hs Code.:

Synonyms:methyl (4-acetylamino-5-{[(2S)-3-(5-chloro-1'H,3H-spiro[1-benzofuran-2,4'-piperidin]-1'-yl)-2-hydroxypropyl]oxy}phenoxy)acetate

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Chemical Property of methyl (4-acetylamino-5-{[(2S)-3-(5-chloro-1'H,3H-spiro[1-benzofuran-2,4'-piperidin]-1'-yl)-2-hydroxypropyl]oxy}phenoxy)acetate

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Technology Process of methyl (4-acetylamino-5-{[(2S)-3-(5-chloro-1'H,3H-spiro[1-benzofuran-2,4'-piperidin]-1'-yl)-2-hydroxypropyl]oxy}phenoxy)acetate

There total 2 articles about methyl (4-acetylamino-5-{[(2S)-3-(5-chloro-1'H,3H-spiro[1-benzofuran-2,4'-piperidin]-1'-yl)-2-hydroxypropyl]oxy}phenoxy)acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 33.0%

: 644968-75-2
N-(2-{[(2S)-3-(5-chloro-1'H,3H-spiro[1-benzofuran-2,4'-piperidin]-1'-yl)-2-hydroxypropyl]oxy}-4-hydroxyphenyl)acetamide

: 96-32-2
bromoacetic acid methyl ester

: 1003567-22-3
methyl (4-acetylamino-5-{[(2S)-3-(5-chloro-1'H,3H-spiro[1-benzofuran-2,4'-piperidin]-1'-yl)-2-hydroxypropyl]oxy}phenoxy)acetate

Guidance literature:: With caesium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 6h; Product distribution / selectivity;

Reference yield:

: 96-32-2
bromoacetic acid methyl ester

: 1003567-22-3
methyl (4-acetylamino-5-{[(2S)-3-(5-chloro-1'H,3H-spiro[1-benzofuran-2,4'-piperidin]-1'-yl)-2-hydroxypropyl]oxy}phenoxy)acetate

Guidance literature:: N-[2-[(2S)-3-(5-chlorospiro[benzofuran-2(3H),4'-piperidin]-1'-yl)-2-hydroxypropoxy]-4-hydroxyphenyl]acetamide trifluoroacetic acid salt; With sodium hydride; In tetrahydrofuran; for 0.5h;

bromoacetic acid methyl ester; In tetrahydrofuran; at 20 ℃; for 20h; Product distribution / selectivity;