methyl 3-chloro-4-(3-(3-phenyl-7-propylbenzofuran-6-yloxy)propylthio)-phenylacetate

Base Information

Chemical Name:methyl 3-chloro-4-(3-(3-phenyl-7-propylbenzofuran-6-yloxy)propylthio)-phenylacetate
CAS No.:194608-93-0
Molecular Formula:C₂₉H₂₉ClO₄S
Molecular Weight:509.066
Hs Code.:

Synonyms:methyl 3-chloro-4-(3-(3-phenyl-7-propylbenzofuran-6-yloxy)propylthio)-phenylacetate

Suppliers and Price of methyl 3-chloro-4-(3-(3-phenyl-7-propylbenzofuran-6-yloxy)propylthio)-phenylacetate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of methyl 3-chloro-4-(3-(3-phenyl-7-propylbenzofuran-6-yloxy)propylthio)-phenylacetate

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of methyl 3-chloro-4-(3-(3-phenyl-7-propylbenzofuran-6-yloxy)propylthio)-phenylacetate

There total 13 articles about methyl 3-chloro-4-(3-(3-phenyl-7-propylbenzofuran-6-yloxy)propylthio)-phenylacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3-chloro-4-dimethylcarbomoylthio-benzene-acetic acid, methyl ester

: 194608-92-9
3-phenyl-6-(3-bromopropyloxy)-7-propylbenzofuran

: 194608-93-0
methyl 3-chloro-4-(3-(3-phenyl-7-propylbenzofuran-6-yloxy)propylthio)-phenylacetate

Guidance literature:: With sodium methylate; In methanol; hexane; dichloromethane;

Reference yield:

: 150-19-6
O-methylresorcine

: 194608-93-0
methyl 3-chloro-4-(3-(3-phenyl-7-propylbenzofuran-6-yloxy)propylthio)-phenylacetate

Guidance literature:: Multi-step reaction with 7 steps

1: Cs₂CO₃ / dimethylformamide

2: CH₃SO₂OH / CH₂Cl₂ / -10 - 20 °C

3: BBr₃ / CH₂Cl₂ / 1 h / -10 - 20 °C

4: Cs₂CO₃ / dimethylformamide

5: 1,2-dichloro-benzene / Heating

6: H₂ / 5 percent Pd/C / various solvent(s) / 0.5 h / 760 Torr

7: Cs₂CO₃ / dimethylformamide

With methanesulfonic acid; hydrogen; boron tribromide; caesium carbonate; palladium on activated charcoal; In dichloromethane; N,N-dimethyl-formamide; 1,2-dichloro-benzene; 5: Claisen rearrangement;
DOI:10.1016/S0960-894X(03)00115-X

Reference yield:

: 13196-08-2
3-phenyl-benzofuran-6-ol

: 194608-93-0
methyl 3-chloro-4-(3-(3-phenyl-7-propylbenzofuran-6-yloxy)propylthio)-phenylacetate

Guidance literature:: Multi-step reaction with 4 steps

1: Cs₂CO₃ / dimethylformamide

2: 1,2-dichloro-benzene / Heating

3: H₂ / 5 percent Pd/C / various solvent(s) / 0.5 h / 760 Torr

4: Cs₂CO₃ / dimethylformamide

With hydrogen; caesium carbonate; palladium on activated charcoal; In N,N-dimethyl-formamide; 1,2-dichloro-benzene; 2: Claisen rearrangement;
DOI:10.1016/S0960-894X(03)00115-X