C₂₂H₁₈N₂O₆

Base Information

Chemical Name:C₂₂H₁₈N₂O₆
CAS No.:161391-22-6
Molecular Formula:C₂₂H₁₈N₂O₆
Molecular Weight:406.395
Hs Code.:

C<sub>22</sub>H<sub>18</sub>N<sub>2</sub>O<sub>6</sub>

Synonyms:C₂₂H₁₈N₂O₆

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Chemical Property of C₂₂H₁₈N₂O₆

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Technology Process of C₂₂H₁₈N₂O₆

There total 4 articles about C₂₂H₁₈N₂O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 161391-19-1
C₂₁H₂₀N₂O₆

: 161391-22-6
C₂₂H₁₈N₂O₆

Guidance literature:: Multi-step reaction with 3 steps

1: 86 percent / di-isopropyl-D-tartrate, 4A molecular sieves, titanium tetraisopropoxide, t-butyl hydroperoxide / CH₂Cl₂ / 14 h / 0 °C

2: 99 percent / Dess-Martin periodinane / CH₂Cl₂ / 36 h / 25 °C

3: 57 percent / 1.) n-butyl lithium / tetrahydrofuran; hexane / 1.) -78 deg C, 0.25 h; 2.) 0 deg C, 3 h

With titanium(IV) isopropylate; tert.-butylhydroperoxide; n-butyllithium; 4 A molecular sieve; Dess-Martin periodane; diisopropyl-d₀ D-tartrate; In tetrahydrofuran; hexane; dichloromethane;
DOI:10.1016/S0040-4020(01)89281-4

Reference yield:

: 161391-20-4
C₂₁H₂₀N₂O₇

: 161391-22-6
C₂₂H₁₈N₂O₆

Guidance literature:: Multi-step reaction with 2 steps

1: 99 percent / Dess-Martin periodinane / CH₂Cl₂ / 36 h / 25 °C

2: 57 percent / 1.) n-butyl lithium / tetrahydrofuran; hexane / 1.) -78 deg C, 0.25 h; 2.) 0 deg C, 3 h

With n-butyllithium; Dess-Martin periodane; In tetrahydrofuran; hexane; dichloromethane;
DOI:10.1016/S0040-4020(01)89281-4

Reference yield:

: 161391-16-8
C₂₇H₃₆N₂O₇Si

: 161391-22-6
C₂₂H₁₈N₂O₆

Guidance literature:: Multi-step reaction with 5 steps

1: 75 percent / triethylamine, DMAP, trifluoroacetic anhydride / CH₂Cl₂ / 0.25 h / 25 °C

2: 96 percent / hydrogen fluoride/pyridine / tetrahydrofuran / 1 h / 0 °C

3: 86 percent / di-isopropyl-D-tartrate, 4A molecular sieves, titanium tetraisopropoxide, t-butyl hydroperoxide / CH₂Cl₂ / 14 h / 0 °C

4: 99 percent / Dess-Martin periodinane / CH₂Cl₂ / 36 h / 25 °C

5: 57 percent / 1.) n-butyl lithium / tetrahydrofuran; hexane / 1.) -78 deg C, 0.25 h; 2.) 0 deg C, 3 h

With pyridine; titanium(IV) isopropylate; tert.-butylhydroperoxide; dmap; n-butyllithium; 4 A molecular sieve; hydrogen fluoride; Dess-Martin periodane; diisopropyl-d₀ D-tartrate; triethylamine; trifluoroacetic anhydride; In tetrahydrofuran; hexane; dichloromethane;
DOI:10.1016/S0040-4020(01)89281-4