(R)-<2-<(2-Hydroxyethyl)(phenylmethyl)amino>-1-methyl-2-oxoethyl>carbamic acid 1,1-dimethylethyl ester

Base Information

Chemical Name:(R)-<2-<(2-Hydroxyethyl)(phenylmethyl)amino>-1-methyl-2-oxoethyl>carbamic acid 1,1-dimethylethyl ester
CAS No.:170033-53-1
Molecular Formula:C₁₇H₂₆N₂O₄
Molecular Weight:322.404
Hs Code.:

Synonyms:(R)-<2-<(2-Hydroxyethyl)(phenylmethyl)amino>-1-methyl-2-oxoethyl>carbamic acid 1,1-dimethylethyl ester

Suppliers and Price of (R)-<2-<(2-Hydroxyethyl)(phenylmethyl)amino>-1-methyl-2-oxoethyl>carbamic acid 1,1-dimethylethyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of (R)-<2-<(2-Hydroxyethyl)(phenylmethyl)amino>-1-methyl-2-oxoethyl>carbamic acid 1,1-dimethylethyl ester

Chemical Property:

Purity/Quality:: 99% ^*data from raw suppliers

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Technology Process of (R)-<2-<(2-Hydroxyethyl)(phenylmethyl)amino>-1-methyl-2-oxoethyl>carbamic acid 1,1-dimethylethyl ester

There total 1 articles about (R)-<2-<(2-Hydroxyethyl)(phenylmethyl)amino>-1-methyl-2-oxoethyl>carbamic acid 1,1-dimethylethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3744-87-4,7764-95-6,15761-38-3
Boc-(R)-Ala

: 104-63-2
N-Benzylethanolamine

: 170033-53-1
(R)-<2-<(2-Hydroxyethyl)(phenylmethyl)amino>-1-methyl-2-oxoethyl>carbamic acid 1,1-dimethylethyl ester

Guidance literature:: With 1,1'-carbonyldiimidazole; Yield given. Multistep reaction; 1.) THF, room temp., 1 h, 2.) THF, room temp., 16 h;
DOI:10.1021/jo00118a039

Reference yield:

: 170033-53-1
(R)-<2-<(2-Hydroxyethyl)(phenylmethyl)amino>-1-methyl-2-oxoethyl>carbamic acid 1,1-dimethylethyl ester

: 170033-65-5
(R)-2-Amino-N-benzyl-N-(2-hydroxy-ethyl)-propionamide

Guidance literature:: With trifluoroacetic acid; In dichloromethane; at 0 ℃; for 1.75h;
DOI:10.1021/jo00118a039

Reference yield:

: 170033-53-1
(R)-<2-<(2-Hydroxyethyl)(phenylmethyl)amino>-1-methyl-2-oxoethyl>carbamic acid 1,1-dimethylethyl ester

: 132871-11-5
(R)-3-Methyl-1-(phenylmethyl)piperazine

Guidance literature:: Multi-step reaction with 3 steps

1: TFA / CH₂Cl₂ / 1.75 h / 0 °C

2: DEAD, PPh₃ / tetrahydrofuran / 16 h / Ambient temperature

3: LAH / tetrahydrofuran / 16 h / Heating

With lithium aluminium tetrahydride; triphenylphosphine; trifluoroacetic acid; diethylazodicarboxylate; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jo00118a039