C₂₄H₂₃NO₃

Base Information

Chemical Name:C₂₄H₂₃NO₃
CAS No.:1447728-86-0
Molecular Formula:C₂₄H₂₃NO₃
Molecular Weight:373.452
Hs Code.:

C<sub>24</sub>H<sub>23</sub>NO<sub>3</sub>

Synonyms:C₂₄H₂₃NO₃

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Chemical Property of C₂₄H₂₃NO₃

Chemical Property:

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Technology Process of C₂₄H₂₃NO₃

There total 7 articles about C₂₄H₂₃NO₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3956-07-8
4-iodobenzamide

: 1447729-00-1
C₁₇H₁₇BrO₂Zn

: 1447728-86-0
C₂₄H₂₃NO₃

Guidance literature:: With dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; palladium diacetate; at 20 ℃; for 27h; Inert atmosphere;
DOI:10.1016/j.tetlet.2013.05.114

Reference yield:

: C₁₆H₁₈Se

: 1447728-86-0
C₂₄H₂₃NO₃

Guidance literature:: Multi-step reaction with 5 steps

1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 1 h / -78 °C / Inert atmosphere

2: sodium benzoate / toluene / 1 h / 100 °C / Inert atmosphere

3: Phenylselenyl bromide / dichloromethane / 5 h / -45 - 0 °C / Inert atmosphere

4: lithium; naphthalene; trimethylsilyl bromide / tetrahydrofuran / 19 h / 20 °C / Inert atmosphere; Sonication

5: palladium diacetate; dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane / 27 h / 20 °C / Inert atmosphere

With dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; sodium benzoate; naphthalene; trimethylsilyl bromide; Phenylselenyl bromide; palladium diacetate; lithium; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; dichloromethane; toluene;
DOI:10.1016/j.tetlet.2013.05.114

Reference yield:

: 1447728-69-9
C₂₃H₂₂O₂Se

: 1447728-86-0
C₂₄H₂₃NO₃

Guidance literature:: Multi-step reaction with 3 steps

1: Phenylselenyl bromide / dichloromethane / 5 h / -45 - 0 °C / Inert atmosphere

2: lithium; naphthalene; trimethylsilyl bromide / tetrahydrofuran / 19 h / 20 °C / Inert atmosphere; Sonication

3: palladium diacetate; dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane / 27 h / 20 °C / Inert atmosphere

With dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; naphthalene; trimethylsilyl bromide; Phenylselenyl bromide; palladium diacetate; lithium; In tetrahydrofuran; dichloromethane;
DOI:10.1016/j.tetlet.2013.05.114