5-O-2,3-di-O-benzoyl-β-D-ribofuranoside

Base Information

• Chemical Name: 5-O-2,3-di-O-benzoyl-β-D-ribofuranoside
• CAS No.: 77886-97-6
• Molecular Formula: C₃₂H₃₄O₁₆
• Molecular Weight: 674.612

Synonyms:5-O-2,3-di-O-benzoyl-β-D-ribofuranoside

Chemical Property of 5-O-2,3-di-O-benzoyl-β-D-ribofuranoside

Chemical Property:

Purity/Quality:

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Technology Process of 5-O-2,3-di-O-benzoyl-β-D-ribofuranoside

There total 1 articles about 5-O-2,3-di-O-benzoyl-β-D-ribofuranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C26H24O7 (77886-95-4) → 5-O-2,3-di-O-benzoyl-β-D-ribofuranoside (77886-97-6)

Guidance literature:

Multi-step reaction with 2 steps

1: 36.6 percent / Hg(CN)2 / nitromethane; benzene; CH₂Cl₂ / 4 h / Heating

2: 76 percent / H₂ / 10percent Pd/C / acetic acid; H₂O / 120 h / 2128 Torr

With hydrogen; mercury(II) cyanide; palladium on activated charcoal; In nitromethane; dichloromethane; water; acetic acid; benzene;

DOI:10.1021/jm00139a026

Reference yield:

tris(trimethylsilyl)-5-fluorocytosine + 5-O-2,3-di-O-benzoyl-β-D-ribofuranoside (77886-97-6) → 2',3'-di-O-benzoyl-5'-O-(methyl 2'',3'',4''-tri-O-acetyl-β-D-glucopyranosyluronate)-5-fluorocytidine

Guidance literature:

With triphenylphosphine; Yield given. Multistep reaction; 1.) MeCN, CCl₄, reflux, 3 h, 2.) MeCN, reflux, 24 h;

DOI:10.1021/jm00139a026

upstream raw materials:

C₂₆H₂₄O₇

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